2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranosyl 2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranoside

Base Information

Chemical Name:2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranosyl 2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranoside
CAS No.:216572-30-4
Molecular Formula:C₄₈H₄₆N₄O₁₁S₂
Molecular Weight:919.045
Hs Code.:

2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranosyl 2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranoside

Synonyms:2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranosyl 2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranoside

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Chemical Property of 2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranosyl 2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranoside

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Technology Process of 2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranosyl 2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranoside

There total 1 articles about 2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranosyl 2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 127128-54-5
2-O-benzyl-4,6-O-(R)-benzylidene-α-D-glucopyranosyl 2-O-benzyl-4,6-O-(R)-benzylidene-α-D-glucopyranoside

: 6160-65-2
1,1'-Thiocarbonyldiimidazole

: 216572-30-4
2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranosyl 2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranoside

Guidance literature:: With dmap; In acetonitrile; for 65h; Heating;
DOI:10.1080/07328309808001900

Reference yield: 66.0%

: 216572-30-4
2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranosyl 2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranoside

: 216572-31-5
2-O-benzyl-4,6-O-(R)-benzylidene-3-deoxy-α-D-ribo-hexopyranosyl 2-O-benzyl-4,6-O-(R)-benzylidene-3-deoxy-α-D-ribo-hexopyranoside

Guidance literature:: With azobisisobutyronitrile; tri-n-butyl-tin hydride; In toluene; for 16h; Heating;
DOI:10.1080/07328309808001900

Reference yield:

: 216572-30-4
2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranosyl 2-O-benzyl-4,6-O-(R)-benzylidene-3-O-(imidazol-1-yl-thiocarbonyl)-α-D-glucopyranoside

: 216572-34-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl-(1-4)-O-(2,3,6-tri-O-acetyl-β-D-glucopyranosyl)-(1-4)-2,6-di-O-benzyl-3-deoxy-α-D-ribo-hexopyranosyl 2-O-benzyl-4,6-O-(R)-benzylidene-α-D-ribo-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / α,α'-azodiisobutyronitrile; tributyltin hydride / toluene / 16 h / Heating

2: 32 percent / sodium cyanoborohydride; hydrochloric acid / tetrahydrofuran; diethyl ether

3: 46 percent / tetramethylurea; silver triflate / CH₂Cl₂ / 18 h / 20 °C

With hydrogenchloride; azobisisobutyronitrile; tri-n-butyl-tin hydride; silver trifluoromethanesulfonate; sodium cyanoborohydride; tetramethylurea; In tetrahydrofuran; diethyl ether; dichloromethane; toluene; 1: Reduction / 2: Ring cleavage / 3: Condensation;
DOI:10.1080/07328309808001900