1-O-(3,4-Dimethoxybenzyl)-2,3-di-O-[3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraen-1-yl]-sn-glycerol

Base Information

Chemical Name:1-O-(3,4-Dimethoxybenzyl)-2,3-di-O-[3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraen-1-yl]-sn-glycerol
CAS No.:264187-57-7
Molecular Formula:C₅₂H₈₂O₅
Molecular Weight:787.22
Hs Code.:

Synonyms:1-O-(3,4-Dimethoxybenzyl)-2,3-di-O-[3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraen-1-yl]-sn-glycerol

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Chemical Property of 1-O-(3,4-Dimethoxybenzyl)-2,3-di-O-[3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraen-1-yl]-sn-glycerol

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Technology Process of 1-O-(3,4-Dimethoxybenzyl)-2,3-di-O-[3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraen-1-yl]-sn-glycerol

There total 10 articles about 1-O-(3,4-Dimethoxybenzyl)-2,3-di-O-[3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraen-1-yl]-sn-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 68799-82-6
1-chloro-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraene

: 139115-87-0
2(R)-3-((3,4-dimethoxybenzyl)oxy)propane-1,2-diol

: C₃₂H₅₀O₅

: 264187-57-7
1-O-(3,4-Dimethoxybenzyl)-2,3-di-O-[3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraen-1-yl]-sn-glycerol

Guidance literature:: 2(R)-3-((3,4-dimethoxybenzyl)oxy)propane-1,2-diol; With sodium hydride; In dimethyl sulfoxide; at 21 ℃; for 1h; Schlenk technique;

1-chloro-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraene; In dimethyl sulfoxide; for 16h; Schlenk technique;
DOI:10.1016/j.chembiol.2014.07.022

Reference yield: 60.0%

: 68799-82-6
1-chloro-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraene

: 1-O-(3,4-Dimethoxybenzyl)-sn-glycerol

: 264187-57-7
1-O-(3,4-Dimethoxybenzyl)-2,3-di-O-[3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraen-1-yl]-sn-glycerol

Guidance literature:: 1-O-(3,4-Dimethoxybenzyl)-sn-glycerol; With sodium hydride; In dimethyl sulfoxide; for 2h;

1-chloro-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraene; In dimethyl sulfoxide; at 20 ℃;

Reference yield:

: 7306-46-9
4-chloromethyl-1,2-dimethoxy-benzene

: C₃₂H₅₀O₅

: 264187-57-7
1-O-(3,4-Dimethoxybenzyl)-2,3-di-O-[3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraen-1-yl]-sn-glycerol

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetra-(n-butyl)ammonium iodide; potassium hydride / tetrahydrofuran; paraffin oil / 0.17 h / Schlenk technique; Inert atmosphere

1.2: 16 h / Schlenk technique; Inert atmosphere; Reflux

2.1: Amberlite IR₁₂₀ (acidform) / dichloromethane; methanol / 36 h / 21 °C / Schlenk technique

3.1: sodium hydride / dimethyl sulfoxide / 1 h / 21 °C / Schlenk technique

3.2: 16 h / Schlenk technique

With tetra-(n-butyl)ammonium iodide; potassium hydride; sodium hydride; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; paraffin oil;
DOI:10.1016/j.chembiol.2014.07.022