diphenylacetic acid-1-13C

Base Information

Chemical Name:diphenylacetic acid-1-13C
CAS No.:106627-09-2
Molecular Formula:C₁₄H₁₂O₂
Molecular Weight:213.237
Hs Code.:

Synonyms:diphenylacetic acid-1-13C

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Chemical Property of diphenylacetic acid-1-13C

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Technology Process of diphenylacetic acid-1-13C

There total 3 articles about diphenylacetic acid-1-13C which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1111-72-4
carbon dioxide

: potassium diphenylacetate

: 106627-09-2
diphenylacetic acid-1-13C

Guidance literature:: In N,N-dimethyl-formamide; at 90 ℃; for 2h; under 760.051 Torr;
DOI:10.1126/science.abb4129

Reference yield: 75.0%

: 117-34-0
2,2-diphenylacetic acid

: 1111-72-4
carbon dioxide

: 106627-09-2
diphenylacetic acid-1-13C

Guidance literature:: With (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; caesium carbonate; In N,N-dimethyl acetamide; at 20 ℃; for 0.5h; under 760.051 Torr; Glovebox; Inert atmosphere; Sealed tube; Irradiation;
DOI:10.1021/jacs.0c12819

Reference yield: 65.0%

: 101-81-5
Diphenylmethane

: 1111-72-4
carbon dioxide

: 106627-09-2
diphenylacetic acid-1-13C

Guidance literature:: Diphenylmethane; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; for 14h; Heating;

carbon dioxide; In hexane; for 20h; under 760.051 Torr; Further stages.;
DOI:10.1021/ja004324z