C₁₈H₁₆Cl₂SiZn₂

Base Information

• Chemical Name: C₁₈H₁₆Cl₂SiZn₂
• CAS No.: 333174-61-1
• Molecular Formula: C₁₈H₁₆Cl₂SiZn₂
• Molecular Weight: 462.097
• Mol file: 333174-61-1.mol

Synonyms:C₁₈H₁₆Cl₂SiZn₂

Chemical Property of C₁₈H₁₆Cl₂SiZn₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₁₈H₁₆Cl₂SiZn₂

There total 7 articles about C₁₈H₁₆Cl₂SiZn₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dichloro(N,N,N’,N‘-tetramethylethylenediamine)zinc + dimethylbis(phenylethynyl)silane (2170-08-3) → C18H16Cl2SiZn2 (333174-61-1)

Guidance literature:

dimethylbis(phenylethynyl)silane; With naphthalene; lithium; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

dichloro(N,N,N’,N‘-tetramethylethylenediamine)zinc; In tetrahydrofuran; at -10 - 20 ℃; for 1h; Inert atmosphere;

DOI:10.1039/c2jm34621d

Reference yield:

2,5-dilithium-3,4-diphenyl-1,1-dimethylsilole (160319-30-2) → C18H16Cl2SiZn2 (333174-61-1)

Guidance literature:

With dichloro(N,N,N’,N‘-tetramethylethylenediamine)zinc; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1021/ma902432m

Reference yield:

zinc dichloro(N,N,N′,N′-tetramethylethylenediamine) (28308-00-1) + dimethylbis(phenylethynyl)silane (2170-08-3) → C18H16Cl2SiZn2 (333174-61-1)

Guidance literature:

dimethylbis(phenylethynyl)silane; With naphthalene; lithium; In tetrahydrofuran; for 0.583333h; Inert atmosphere; Schlenk technique;

zinc dichloro(N,N,N′,N′-tetramethylethylenediamine); In tetrahydrofuran; at 0 - 20 ℃; for 1.5h; Time; Inert atmosphere; Schlenk technique; Sonication;

DOI:10.1021/om400022f

upstream raw materials:

2,5-dilithium-3,4-diphenyl-1,1-dimethylsilole

dimethylbis(phenylethynyl)silane

zinc dichloro(N,N,N′,N′-tetramethylethylenediamine)

zinc(II) chloride

Downstream raw materials:

1,1-dimethyl-2,5-bis(4'-bromophenyl)-3,4-diphenylsilole

2,5-bis[3,4-bis(methylthio)phenyl]-1,1-dimethyl-3,4-diphenylsilole

1,1-dimethyl-2,5-bis(2,2′-bipyridin-6-yl)-3,4-diphenylsilole

C₆₄H₄₆Si₂