2-[(Z)-2-[2-[(Z)-2-(aminocarbonyl)hydrazono]-2-(4-methylphenyl)ethyl]disulfanyl-1-(4-methylphenyl)ethylidene]-1-hydrazinecarboxamide

Base Information

Chemical Name:2-[(Z)-2-[2-[(Z)-2-(aminocarbonyl)hydrazono]-2-(4-methylphenyl)ethyl]disulfanyl-1-(4-methylphenyl)ethylidene]-1-hydrazinecarboxamide
CAS No.:1277181-63-1
Molecular Formula:C₂₀H₂₄N₆O₂S₂
Molecular Weight:444.582
Hs Code.:

Synonyms:2-[(Z)-2-[2-[(Z)-2-(aminocarbonyl)hydrazono]-2-(4-methylphenyl)ethyl]disulfanyl-1-(4-methylphenyl)ethylidene]-1-hydrazinecarboxamide

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Chemical Property of 2-[(Z)-2-[2-[(Z)-2-(aminocarbonyl)hydrazono]-2-(4-methylphenyl)ethyl]disulfanyl-1-(4-methylphenyl)ethylidene]-1-hydrazinecarboxamide

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Technology Process of 2-[(Z)-2-[2-[(Z)-2-(aminocarbonyl)hydrazono]-2-(4-methylphenyl)ethyl]disulfanyl-1-(4-methylphenyl)ethylidene]-1-hydrazinecarboxamide

There total 2 articles about 2-[(Z)-2-[2-[(Z)-2-(aminocarbonyl)hydrazono]-2-(4-methylphenyl)ethyl]disulfanyl-1-(4-methylphenyl)ethylidene]-1-hydrazinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 325850-77-9
2-(4,5-dihydro-1,3-thiazol-2-ylsulfanyl)-1-(4-methylphenyl)-1-ethanone

: 563-41-7
semicarbazide hydrochloride

: 1277181-63-1
2-[(Z)-2-[2-[(Z)-2-(aminocarbonyl)hydrazono]-2-(4-methylphenyl)ethyl]disulfanyl-1-(4-methylphenyl)ethylidene]-1-hydrazinecarboxamide

Guidance literature:: With tetrabutylammomium bromide; sodium acetate; In 1,4-dioxane; water; at 20 ℃; for 72h;
DOI:10.1080/17415993.2010.533772

Reference yield:

: 619-41-0
4-(bromoacetyl)toluene

: 1277181-63-1
2-[(Z)-2-[2-[(Z)-2-(aminocarbonyl)hydrazono]-2-(4-methylphenyl)ethyl]disulfanyl-1-(4-methylphenyl)ethylidene]-1-hydrazinecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / ethanol; N,N-dimethyl-formamide / 2 h

2: tetrabutylammomium bromide; sodium acetate / 1,4-dioxane; water / 72 h / 20 °C

With tetrabutylammomium bromide; sodium acetate; triethylamine; In 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1080/17415993.2010.533772