acetamide, N-(4-tricyclo[3.3.1.1~3,7~]dec-1-ylphenyl)-

Base Information

• Chemical Name: acetamide, N-(4-tricyclo[3.3.1.1~3,7~]dec-1-ylphenyl)-
• CAS No.: 1459-50-3
• Molecular Formula: C₁₈H₂₃NO
• Molecular Weight: 269.387
• Mol file: 1459-50-3.mol

Synonyms:N-(4-((3r,5r,7r)-adamantan-1-yl)phenyl)acetamide

Chemical Property of acetamide, N-(4-tricyclo[3.3.1.1~3,7~]dec-1-ylphenyl)-

Chemical Property:

• Melting Point: 173-175 °C
• Boiling Point: 448.6±24.0 °C(Predicted)
• PKA: 15.07±0.70(Predicted)
• Density: 1.163±0.06 g/cm3(Predicted)
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

N-[4-(1-Adamantyl)phenyl]acetamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of acetamide, N-(4-tricyclo[3.3.1.1~3,7~]dec-1-ylphenyl)-

There total 4 articles about acetamide, N-(4-tricyclo[3.3.1.1~3,7~]dec-1-ylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

1-Adamantyl bromide (768-90-1) + Acetanilid (103-84-4) → N-(4-((3r,5r,7r)-adamantan-1-yl)phenyl)acetamide (1459-50-3)

Guidance literature:

With zinc(II) chloride; at 75 ℃;

DOI:10.1007/s10593-008-0136-z

Reference yield:

adamantane (281-23-2) + Acetanilid (103-84-4) → 1-adamantanol (700-57-2) + N-(4-((3r,5r,7r)-adamantan-1-yl)phenyl)acetamide (1459-50-3)

Guidance literature:

With sulfuric acid; trifluoroacetic anhydride; Yield given. Multistep reaction; 1) 65 deg C, 3 h, 2) 80 deg C, 1.5 h;

Reference yield:

1-adamanthanol (768-95-6) + Acetanilid (103-84-4) → N-(4-((3r,5r,7r)-adamantan-1-yl)phenyl)acetamide (1459-50-3)

Guidance literature:

With trifluoroacetic acid; at 80 ℃; for 3h;

DOI:10.1007/s11172-020-2873-9

upstream raw materials:

1-Adamantyl bromide

Acetanilid

4-(tricyclo[3.3.1.1^3,7]dec-1-yl)aniline

acetyl chloride

Downstream raw materials:

4-(tricyclo[3.3.1.1^3,7]dec-1-yl)aniline

2-Brom-4--acetanilid

1-(4-acetamido-3-nitrophenyl)adamantane

1-(3-chlorophenyl)tricyclo<3.3.1.1^3,7>decane

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