4-methyl-N-(prop-2-en-1-yl)aniline

Base Information

• Chemical Name: 4-methyl-N-(prop-2-en-1-yl)aniline
• CAS No.: 15258-46-5
• Molecular Formula: C10H13 N
• Molecular Weight: 147.22
• Mol file: 15258-46-5.mol

Synonyms:Benzenamine,4-methyl-N-2-propenyl- (9CI); p-Toluidine, N-allyl- (6CI,8CI);Allyl(4-tolyl)amine; NSC 60288

Chemical Property of 4-methyl-N-(prop-2-en-1-yl)aniline

Chemical Property:

• Vapor Pressure: 0.0493mmHg at 25°C
• Boiling Point: 235.7°Cat760mmHg
• Flash Point: 96°C
• Density: 0.96g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-methyl-N-(prop-2-en-1-yl)aniline

There total 19 articles about 4-methyl-N-(prop-2-en-1-yl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

vinyl magnesium bromide (1826-67-1) + (3-Methyl-indazol-1-ylmethyl)-p-tolyl-amine (156704-05-1) → N-allyl-p-toluidine (15258-46-5)

Guidance literature:

In diethyl ether;

Reference yield: 91.0%

p-toluidine (106-49-0,12221-03-3) + allyl bromide (106-95-6) → N-allyl-p-toluidine (15258-46-5)

Guidance literature:

allyl bromide; With potassium carbonate; In water; at 20 ℃; for 0.0166667h;

p-toluidine; With palladium; In water; at 20 - 65 ℃; for 5h; Time; regioselective reaction;

DOI:10.1002/cctc.201500300

Reference yield: 91.0%

N-allyl-N-(4-methylphenyl)-2-nitrobenzenesulfonamide (1172142-53-8) → N-allyl-p-toluidine (15258-46-5)

Guidance literature:

With potassium carbonate; thiophenol; In N,N-dimethyl-formamide; at 40 ℃; for 4h;

DOI:10.1002/ejoc.200900113

upstream raw materials:

allyl benzenesulfonate

p-toluidine

vinyl magnesium bromide

(3-Methyl-indazol-1-ylmethyl)-p-tolyl-amine

Downstream raw materials:

2-bromo-4-methyl-N-allylaniline

N-allyl-N'-phenyl-N-p-tolyl-thiourea

N-allyl-N-benzyl-4-methylaniline

10-methyl-1-(p-tolyl)-2,3,3a,3b,4,5,6,11b-octahydro-1H-dipyrrolo[1,2-a:3′,2′-c]quinoline

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