N-(2,6-diisopropylphenyl)-6-(2,4,6-triisopropylphenyl)pyridine-2-amine bis(trimethylsilylmethyl)scandium tetrahydrofuranate

Base Information

Chemical Name:N-(2,6-diisopropylphenyl)-6-(2,4,6-triisopropylphenyl)pyridine-2-amine bis(trimethylsilylmethyl)scandium tetrahydrofuranate
CAS No.:1218909-46-6
Molecular Formula:C₄₄H₇₃N₂OScSi₂
Molecular Weight:747.203
Hs Code.:

Synonyms:N-(2,6-diisopropylphenyl)-6-(2,4,6-triisopropylphenyl)pyridine-2-amine bis(trimethylsilylmethyl)scandium tetrahydrofuranate

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Chemical Property of N-(2,6-diisopropylphenyl)-6-(2,4,6-triisopropylphenyl)pyridine-2-amine bis(trimethylsilylmethyl)scandium tetrahydrofuranate

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Technology Process of N-(2,6-diisopropylphenyl)-6-(2,4,6-triisopropylphenyl)pyridine-2-amine bis(trimethylsilylmethyl)scandium tetrahydrofuranate

There total 2 articles about N-(2,6-diisopropylphenyl)-6-(2,4,6-triisopropylphenyl)pyridine-2-amine bis(trimethylsilylmethyl)scandium tetrahydrofuranate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 41705-65-1
[scandium tris(trimethylsilylmethyl)(THF)2]

: 833453-23-9
N-(2,6-diisopropylphenyl)-[6-(2,4,6-triisopropylphenyl)pyridin-2-yl]amine

: 1218909-46-6
N-(2,6-diisopropylphenyl)-6-(2,4,6-triisopropylphenyl)pyridine-2-amine bis(trimethylsilylmethyl)scandium tetrahydrofuranate

Guidance literature:: In hexane; byproducts: Si(CH3)4; (Ar), to a mixt. of Sc complex and ligand (1:1) added hexane at room temp., stirred for 1 h; filtered, evapd.(vac.), elem. anal.;
DOI:10.1002/ejic.200900504

Reference yield:

: (N-(2,6-diisopropylphenyl)-6-(2,4,6-triisopropylphenyl)pyridine-2-amine)ScCl₂(THF)_n

: 1822-00-0
trimethylsilylmethyllithium

: 1218909-46-6
N-(2,6-diisopropylphenyl)-6-(2,4,6-triisopropylphenyl)pyridine-2-amine bis(trimethylsilylmethyl)scandium tetrahydrofuranate

Guidance literature:: In hexane; at 0 ℃; for 2h; Schlenk technique; Inert atmosphere;
DOI:10.1007/s11172-016-1623-5

Reference yield: 70.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 1218909-46-6
N-(2,6-diisopropylphenyl)-6-(2,4,6-triisopropylphenyl)pyridine-2-amine bis(trimethylsilylmethyl)scandium tetrahydrofuranate

: N,N-dimethylanilinium tetraphenylborate

: 1218909-54-6
[(2,6-diisopropylphenyl)-[6-(2,4,6-triisopropylphenyl)pyridin-2-yl]amine]Sc(CH₂SiMe₃)(THF)2[BPh₄]

Guidance literature:: In tetrahydrofuran; (Ar), Sc complex and (BPh4)(PhNHMe2) (1:1) in THF stirred for 20 min; evapd., washed twice (hexane), dried (vac.), elem. anal.;
DOI:10.1002/ejic.200900504