(E)-N-ethyl-N-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzyl)ethananamine

Base Information

Chemical Name:(E)-N-ethyl-N-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzyl)ethananamine
CAS No.:933986-43-7
Molecular Formula:C₁₉H₃₀BNO₂
Molecular Weight:315.264
Hs Code.:

Synonyms:(E)-N-ethyl-N-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzyl)ethananamine

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Chemical Property of (E)-N-ethyl-N-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzyl)ethananamine

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Technology Process of (E)-N-ethyl-N-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzyl)ethananamine

There total 3 articles about (E)-N-ethyl-N-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzyl)ethananamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1095858-18-6
N-ethyl-N-(4-ethynylbenzyl)ethanamine

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 933986-43-7
(E)-N-ethyl-N-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzyl)ethananamine

Guidance literature:: RuHCl(PPh₃)3; In toluene; at 50 ℃; for 18.25h; Inert atmosphere;

Reference yield: 66.0%

: 149777-85-5
(E)-4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzaldehyde

: 109-89-7
diethylamine

: 933986-43-7
(E)-N-ethyl-N-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzyl)ethananamine

Guidance literature:: (E)-4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzaldehyde; With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃;

diethylamine; With acetic acid; In 1,2-dichloro-ethane; at 20 ℃; for 18h; Inert atmosphere;

Reference yield:

: 63697-96-1
4-Ethynylbenzaldehyde

: 933986-43-7
(E)-N-ethyl-N-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzyl)ethananamine

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; sodium tris(acetoxy)borohydride; triethylamine / 1,2-dichloro-ethane / 18 h / 20 °C / Inert atmosphere

2: (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II) / toluene / 12 h / 50 °C / Inert atmosphere

With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); sodium tris(acetoxy)borohydride; acetic acid; triethylamine; In 1,2-dichloro-ethane; toluene;
DOI:10.1021/jm500537u