C₃₇H₄₄FN₃O₆

Base Information

Chemical Name:C₃₇H₄₄FN₃O₆
CAS No.:1565779-15-8
Molecular Formula:C₃₇H₄₄FN₃O₆
Molecular Weight:645.771
Hs Code.:

C<sub>37</sub>H<sub>44</sub>FN<sub>3</sub>O<sub>6</sub>

Synonyms:C₃₇H₄₄FN₃O₆

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Chemical Property of C₃₇H₄₄FN₃O₆

Chemical Property:

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Technology Process of C₃₇H₄₄FN₃O₆

There total 14 articles about C₃₇H₄₄FN₃O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1058705-94-4
N-tert-butoxycarbonyl-2-amino-8-nonenoic acid dicyclohexylamine salt

: C₂₃H₂₁FN₂O₃*ClH

: 1565779-15-8
C₃₇H₄₄FN₃O₆

Guidance literature:: With N-[(dimethylamino)-1H-1,2,3-triazolo-[4,5-b]pyridin-1-ylmethylene]-N-methylmethanaminium hexafluorophosphate N-oxide; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 847547-91-5
2-chloro-3-hydroxyquinoline-4-carboxylic acid

: 1565779-15-8
C₃₇H₄₄FN₃O₆

Guidance literature:: Multi-step reaction with 13 steps

1.1: methanol; toluene / Cooling with ice

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; ethanol; toluene / 6 h / 100 °C / Sealed tube; Inert atmosphere

3.1: diisobutylaluminium hydride / dichloromethane; toluene / 2.5 h / -78 - 20 °C

4.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C

5.1: tetrahydrofuran / 0 °C

6.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C

7.1: boron tribromide / dichloromethane / 1 h / 20 °C

8.1: pyrrolidine / methanol / 8 h / 100 °C / Molecular sieve; Sealed tube

9.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.75 h / 20 °C

10.1: methanesulfonyl chloride; triethylamine / dichloromethane / 0 - 20 °C

10.2: 36 h / 20 °C

11.1: palladium 10% on activated carbon; hydrogen / ethyl acetate

12.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C

13.1: N-[(dimethylamino)-1H-1,2,3-triazolo-[4,5-b]pyridin-1-ylmethylene]-N-methylmethanaminium hexafluorophosphate N-oxide; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

With pyrrolidine; hydrogenchloride; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; N-[(dimethylamino)-1H-1,2,3-triazolo-[4,5-b]pyridin-1-ylmethylene]-N-methylmethanaminium hexafluorophosphate N-oxide; hydrogen; boron tribromide; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; methanesulfonyl chloride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1565779-06-7
C₁₈H₁₄FNO₃

: 1565779-15-8
C₃₇H₄₄FN₃O₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: diisobutylaluminium hydride / dichloromethane; toluene / 2.5 h / -78 - 20 °C

2.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C

3.1: tetrahydrofuran / 0 °C

4.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C

5.1: boron tribromide / dichloromethane / 1 h / 20 °C

6.1: pyrrolidine / methanol / 8 h / 100 °C / Molecular sieve; Sealed tube

7.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.75 h / 20 °C

8.1: methanesulfonyl chloride; triethylamine / dichloromethane / 0 - 20 °C

8.2: 36 h / 20 °C

9.1: palladium 10% on activated carbon; hydrogen / ethyl acetate

10.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C

11.1: N-[(dimethylamino)-1H-1,2,3-triazolo-[4,5-b]pyridin-1-ylmethylene]-N-methylmethanaminium hexafluorophosphate N-oxide; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

With pyrrolidine; hydrogenchloride; sodium tetrahydroborate; palladium 10% on activated carbon; N-[(dimethylamino)-1H-1,2,3-triazolo-[4,5-b]pyridin-1-ylmethylene]-N-methylmethanaminium hexafluorophosphate N-oxide; hydrogen; boron tribromide; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; methanesulfonyl chloride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;