N-tert-butoxycarbonyl-2-amino-8-nonenoic acid dicyclohexylamine salt

Base Information

Chemical Name:N-tert-butoxycarbonyl-2-amino-8-nonenoic acid dicyclohexylamine salt
CAS No.:1058705-94-4
Molecular Formula:C₁₂H₂₃N*C₁₄H₂₅NO₄
Molecular Weight:452.678
Hs Code.:

Synonyms:N-tert-butoxycarbonyl-2-amino-8-nonenoic acid dicyclohexylamine salt

Suppliers and Price of N-tert-butoxycarbonyl-2-amino-8-nonenoic acid dicyclohexylamine salt

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 4 raw suppliers

Chemical Property of N-tert-butoxycarbonyl-2-amino-8-nonenoic acid dicyclohexylamine salt

Chemical Property:

Melting Point:82-84 °C(Solv: heptane (142-82-5))

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of N-tert-butoxycarbonyl-2-amino-8-nonenoic acid dicyclohexylamine salt

There total 9 articles about N-tert-butoxycarbonyl-2-amino-8-nonenoic acid dicyclohexylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.7%

: 924307-76-6,1427467-46-6
(S)-2-amino-8-nonenoic acid

: 24424-99-5
di-tert-butyl dicarbonate

: 101-83-7
N-cyclohexyl-cyclohexanamine

: 1058705-94-4
N-tert-butoxycarbonyl-2-amino-8-nonenoic acid dicyclohexylamine salt

Guidance literature:: (S)-2-amino-8-nonenoic acid; di-tert-butyl dicarbonate; With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; Cooling with ice;

N-cyclohexyl-cyclohexanamine; In acetonitrile; at 50 ℃; for 0.5h;

Reference yield: 80.0%

: 101-83-7
N-cyclohexyl-cyclohexanamine

: 300831-21-4
(S)-2-(tert-butoxycarbonylamino)non-8-enoic acid

: 1058705-94-4
N-tert-butoxycarbonyl-2-amino-8-nonenoic acid dicyclohexylamine salt

Guidance literature:: In ethanol; at 50 - 70 ℃; for 0.5h;

Reference yield:

: 4117-09-3
7-bromo-hept-1-ene

: 1058705-94-4
N-tert-butoxycarbonyl-2-amino-8-nonenoic acid dicyclohexylamine salt

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate; caesium carbonate / acetonitrile / 24 h / Reflux

2.1: potassium hydroxide / ethanol / 2 h / Reflux

2.2: pH 4 - 5 / Reflux

3.1: citric acid / water / pH 4-5 / Reflux

4.1: sodium hydroxide; cobalt(II) chloride hexahydrate / water / 38.5 °C / Enzymatic reaction

5.1: sodium hydroxide / water; tetrahydrofuran / 20 °C / Cooling with ice

5.2: 0.5 h / 50 °C

With cobalt(II) chloride hexahydrate; potassium carbonate; caesium carbonate; citric acid; potassium hydroxide; sodium hydroxide; In tetrahydrofuran; ethanol; water; acetonitrile;