2-[5-[(pyrimidin-2-ylthio)methyl]-1,3,4-oxadiazol-2-ylthio]-2',4'-dichloroacetophenone

Base Information

Chemical Name:2-[5-[(pyrimidin-2-ylthio)methyl]-1,3,4-oxadiazol-2-ylthio]-2',4'-dichloroacetophenone
CAS No.:1335227-35-4
Molecular Formula:C₁₅H₁₀Cl₂N₄O₂S₂
Molecular Weight:413.308
Hs Code.:

Synonyms:2-[5-[(pyrimidin-2-ylthio)methyl]-1,3,4-oxadiazol-2-ylthio]-2',4'-dichloroacetophenone

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Chemical Property of 2-[5-[(pyrimidin-2-ylthio)methyl]-1,3,4-oxadiazol-2-ylthio]-2',4'-dichloroacetophenone

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Technology Process of 2-[5-[(pyrimidin-2-ylthio)methyl]-1,3,4-oxadiazol-2-ylthio]-2',4'-dichloroacetophenone

There total 2 articles about 2-[5-[(pyrimidin-2-ylthio)methyl]-1,3,4-oxadiazol-2-ylthio]-2',4'-dichloroacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1024561-99-6
C₇H₆N₄OS₂

: 2631-72-3
2,4-dichlorophenacyl bromide

: 1335227-35-4
2-[5-[(pyrimidin-2-ylthio)methyl]-1,3,4-oxadiazol-2-ylthio]-2',4'-dichloroacetophenone

Guidance literature:: In acetone; at 20 ℃; for 8h;
DOI:10.3390/molecules16097662

Reference yield:

: 60458-72-2
ethyl α-[(2-pyrimidyl)thio]acetate

: 1335227-35-4
2-[5-[(pyrimidin-2-ylthio)methyl]-1,3,4-oxadiazol-2-ylthio]-2',4'-dichloroacetophenone

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrazine hydrate / ethanol / 3 h / 20 °C

2.1: potassium hydroxide / ethanol / 10 h / Reflux

2.2: pH 5 - 6

3.1: acetone / 8 h / 20 °C

With hydrazine hydrate; potassium hydroxide; In ethanol; acetone;
DOI:10.3390/molecules16097662