1-(4-(4-tetradecyloxybenzoyloxy)phenyl)-4-(4-(4-tetradecyloxybenzoyloxy)benzoyloxymethyl)-1H-1,2,3-triazole

Base Information

Chemical Name:1-(4-(4-tetradecyloxybenzoyloxy)phenyl)-4-(4-(4-tetradecyloxybenzoyloxy)benzoyloxymethyl)-1H-1,2,3-triazole
CAS No.:1394236-58-8
Molecular Formula:C₅₈H₇₇N₃O₈
Molecular Weight:944.265
Hs Code.:

Synonyms:1-(4-(4-tetradecyloxybenzoyloxy)phenyl)-4-(4-(4-tetradecyloxybenzoyloxy)benzoyloxymethyl)-1H-1,2,3-triazole

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Chemical Property of 1-(4-(4-tetradecyloxybenzoyloxy)phenyl)-4-(4-(4-tetradecyloxybenzoyloxy)benzoyloxymethyl)-1H-1,2,3-triazole

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Technology Process of 1-(4-(4-tetradecyloxybenzoyloxy)phenyl)-4-(4-(4-tetradecyloxybenzoyloxy)benzoyloxymethyl)-1H-1,2,3-triazole

There total 2 articles about 1-(4-(4-tetradecyloxybenzoyloxy)phenyl)-4-(4-(4-tetradecyloxybenzoyloxy)benzoyloxymethyl)-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1394236-23-7
4-azidophenyl 4-tetradecyloxybenzoate

: 1394236-32-8
prop-2-ynyl 4-(4-tetradecyloxybenzoyloxy)benzoate

: 1394236-58-8
1-(4-(4-tetradecyloxybenzoyloxy)phenyl)-4-(4-(4-tetradecyloxybenzoyloxy)benzoyloxymethyl)-1H-1,2,3-triazole

Guidance literature:: With C₃₀H₂₇ClCuN₉O; In tetrahydrofuran; N,N-dimethyl-formamide; at 80 ℃; for 1h; Microwave irradiation;
DOI:10.1039/c2jm33612j

Reference yield:

: prop-2-yn-1-yl 4-hydroxybenzoate

: 1394236-58-8
1-(4-(4-tetradecyloxybenzoyloxy)phenyl)-4-(4-(4-tetradecyloxybenzoyloxy)benzoyloxymethyl)-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 16 h / 20 °C / Inert atmosphere; Cooling with ice

2: C₃₀H₂₇ClCuN₉O / N,N-dimethyl-formamide; tetrahydrofuran / 1 h / 80 °C / Microwave irradiation

With dmap; C₃₀H₂₇ClCuN₉O; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2jm33612j