4-azidophenyl 4-tetradecyloxybenzoate

Base Information

Chemical Name:4-azidophenyl 4-tetradecyloxybenzoate
CAS No.:1394236-23-7
Molecular Formula:C₂₇H₃₇N₃O₃
Molecular Weight:451.609
Hs Code.:

Synonyms:4-azidophenyl 4-tetradecyloxybenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-azidophenyl 4-tetradecyloxybenzoate

Chemical Property:

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Technology Process of 4-azidophenyl 4-tetradecyloxybenzoate

There total 4 articles about 4-azidophenyl 4-tetradecyloxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 24541-43-3
4-azidophenol

: 62443-08-7
4-n-pentadecylbenzoic acid

: 1394236-23-7
4-azidophenyl 4-tetradecyloxybenzoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere; Cooling with ice;
DOI:10.1039/c2jm33612j

Reference yield:

: 24541-43-3
4-azidophenol

: 15872-46-5
4-(tetradecyloxy)benzoic acid

: 1394236-23-7
4-azidophenyl 4-tetradecyloxybenzoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1016/j.dyepig.2017.10.025

Reference yield:

: 123-30-8
4-amino-phenol

: 1394236-23-7
4-azidophenyl 4-tetradecyloxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.67 h / 0 °C

1.2: 1 h / 0 - 20 °C

2.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 16 h / 20 °C / Inert atmosphere; Cooling with ice

With hydrogenchloride; dmap; dicyclohexyl-carbodiimide; sodium nitrite; In dichloromethane; water;
DOI:10.1039/c2jm33612j