phenyl-carbamic acid-[2]thienylmethyl ester

Base Information

Chemical Name:phenyl-carbamic acid-[2]thienylmethyl ester
CAS No.:104294-31-7
Molecular Formula:C₁₂H₁₁NO₂S
Molecular Weight:233.291
Hs Code.:

Synonyms:phenyl-carbamic acid-[2]thienylmethyl ester

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Chemical Property of phenyl-carbamic acid-[2]thienylmethyl ester

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Technology Process of phenyl-carbamic acid-[2]thienylmethyl ester

There total 3 articles about phenyl-carbamic acid-[2]thienylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 495-18-1
Benzohydroxamic acid

: 636-72-6
2-thiophenemethanol

: 104294-31-7
phenyl-carbamic acid-[2]thienylmethyl ester

Guidance literature:: Benzohydroxamic acid; With 2-chloro-1,3-dimethylimidazolinium chloride; triethylamine; In dichloromethane; at 20 ℃; for 0.5h;

(2-furyl)methyl alcohol; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1021/jo990211q

Reference yield:

: 98-03-3
thiophene-2-carbaldehyde

: 104294-31-7
phenyl-carbamic acid-[2]thienylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; carbon monoxide; cobalt (II)-acetate tetrahydrate / 185 °C / 117681 Torr / in Hexan

With carbon monoxide; hydrogen; cobalt(II) acetate;
DOI:10.1021/ja01166a012