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(E)-1-(3,4-difluorophenyl)ethanone O-benzyloxime

Base Information Edit
  • Chemical Name:(E)-1-(3,4-difluorophenyl)ethanone O-benzyloxime
  • CAS No.:1434602-38-6
  • Molecular Formula:C15H13F2NO
  • Molecular Weight:261.271
  • Hs Code.:
  • Mol file:1434602-38-6.mol
(E)-1-(3,4-difluorophenyl)ethanone O-benzyloxime

Synonyms:(E)-1-(3,4-difluorophenyl)ethanone O-benzyloxime

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Chemical Property of (E)-1-(3,4-difluorophenyl)ethanone O-benzyloxime Edit
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Technology Process of (E)-1-(3,4-difluorophenyl)ethanone O-benzyloxime

There total 2 articles about (E)-1-(3,4-difluorophenyl)ethanone O-benzyloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
(E)-1-(3,4-difluorophenyl)ethan-1-one oxime; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 1h;
benzyl bromide; In N,N-dimethyl-formamide; at 20 ℃; for 18h;
DOI:10.1021/jo400371x
Guidance literature:
Multi-step reaction with 2 steps
1.1: hydroxylamine hydrochloride; sodium carbonate / ethanol; water / pH 5 / Reflux
2.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C
2.2: 18 h / 20 °C
With hydroxylamine hydrochloride; sodium hydride; sodium carbonate; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo400371x
Guidance literature:
With borane-THF; C19H23BNO3(1-)*H(1+); In 1,4-dioxane; for 72h; enantioselective reaction; Inert atmosphere;
DOI:10.1021/jo400371x
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