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Technology Process of (C6H4)CHNC6H3(CH(CH3)2)2SO3(1-)*Na(1+)=Na[(C6H4)CHNC6H3(CH(CH3)2)2SO3]

(C6H4)CHNC6H3(CH(CH3)2)2SO3(1-)*Na(1+)=Na[(C6H4)CHNC6H3(CH(CH3)2)2SO3]

Base Information
  • Chemical Name:(C6H4)CHNC6H3(CH(CH3)2)2SO3(1-)*Na(1+)=Na[(C6H4)CHNC6H3(CH(CH3)2)2SO3]
  • CAS No.:1210606-46-4
  • Molecular Formula:C19H22NO3S*Na
  • Molecular Weight:367.444
  • Hs Code.:
(C<sub>6</sub>H<sub>4</sub>)CHNC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2SO<sub>3</sub><sup>(1-)</sup>*Na<sup>(1+)</sup>=Na[(C<sub>6</sub>H<sub>4</sub>)CHNC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2SO<sub>3</sub>]

Synonyms:(C6H4)CHNC6H3(CH(CH3)2)2SO3(1-)*Na(1+)=Na[(C6H4)CHNC6H3(CH(CH3)2)2SO3]

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Chemical Property of (C6H4)CHNC6H3(CH(CH3)2)2SO3(1-)*Na(1+)=Na[(C6H4)CHNC6H3(CH(CH3)2)2SO3]
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Technology Process of (C6H4)CHNC6H3(CH(CH3)2)2SO3(1-)*Na(1+)=Na[(C6H4)CHNC6H3(CH(CH3)2)2SO3]

There total 1 articles about (C6H4)CHNC6H3(CH(CH3)2)2SO3(1-)*Na(1+)=Na[(C6H4)CHNC6H3(CH(CH3)2)2SO3] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

benzaldehyde
100-52-7

benzaldehyde

3,5-diisopropyl sulfanilic acid sodium salt

3,5-diisopropyl sulfanilic acid sodium salt

(C<sub>6</sub>H<sub>4</sub>)CHNC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2SO<sub>3</sub><sup>(1-)</sup>*Na<sup>(1+)</sup>=Na[(C<sub>6</sub>H<sub>4</sub>)CHNC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2SO<sub>3</sub>]
1210606-46-4

(C6H4)CHNC6H3(CH(CH3)2)2SO3(1-)*Na(1+)=Na[(C6H4)CHNC6H3(CH(CH3)2)2SO3]

Guidance literature:
With formic acid; In methanol; at 40 ℃;
DOI:10.1016/j.jorganchem.2009.09.039

Reference yield: 60.0%

lithium tetrachloropalladate

lithium tetrachloropalladate

(C<sub>6</sub>H<sub>4</sub>)CHNC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2SO<sub>3</sub><sup>(1-)</sup>*Na<sup>(1+)</sup>=Na[(C<sub>6</sub>H<sub>4</sub>)CHNC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2SO<sub>3</sub>]
1210606-46-4

(C6H4)CHNC6H3(CH(CH3)2)2SO3(1-)*Na(1+)=Na[(C6H4)CHNC6H3(CH(CH3)2)2SO3]

[(C<sub>6</sub>H<sub>4</sub>)CHNC<sub>6</sub>H<sub>2</sub>(CH(CH<sub>3</sub>)2)2SO<sub>3</sub>PdCl]2<sup>(2-)</sup>*2Na<sup>(1+)</sup>=Na<sub>2</sub>[(C<sub>6</sub>H<sub>4</sub>)CHNC<sub>6</sub>H<sub>2</sub>(CH(CH<sub>3</sub>)2)2SO<sub>3</sub>PdCl]2

[(C6H4)CHNC6H2(CH(CH3)2)2SO3PdCl]2(2-)*2Na(1+)=Na2[(C6H4)CHNC6H2(CH(CH3)2)2SO3PdCl]2

Guidance literature:
With CH3COONa; In methanol; flask with stir bar filled eith Li2PdCl4, Schiff base and CH3COONa underN2; MeOH added; mixt. stirred at room temp. for 2 d; filtered off, recrystd. from MeOH/ethyl ether; elem. anal.;
DOI:10.1016/j.jorganchem.2009.09.039
upstream raw materials:

benzaldehyde

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