(S)-2-(4-fluorophenyl)-1,2,3,4-tetrahydroquinoxaline

Base Information

Chemical Name:(S)-2-(4-fluorophenyl)-1,2,3,4-tetrahydroquinoxaline
CAS No.:1252876-00-8
Molecular Formula:C₁₄H₁₃FN₂
Molecular Weight:228.269
Hs Code.:

Synonyms:(S)-2-(4-fluorophenyl)-1,2,3,4-tetrahydroquinoxaline

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Chemical Property of (S)-2-(4-fluorophenyl)-1,2,3,4-tetrahydroquinoxaline

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Technology Process of (S)-2-(4-fluorophenyl)-1,2,3,4-tetrahydroquinoxaline

There total 4 articles about (S)-2-(4-fluorophenyl)-1,2,3,4-tetrahydroquinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 449-46-7
2-(4-fluorophenyl)quinoxaline

: 1252876-00-8
(S)-2-(4-fluorophenyl)-1,2,3,4-tetrahydroquinoxaline

Guidance literature:: With C₁₇H₂₈N₂O₂RuS⁽¹⁺⁾*C₃₂H₁₂BF₂₄^(1-); hydrogen; In 1,1-dichloroethane; at 20 ℃; for 16h; under 60804.1 Torr; optical yield given as %ee; enantioselective reaction; Autoclave;
DOI:10.1021/ol2029096

Reference yield: 51.0%

: 18511-62-1,53631-23-5,134356-74-4,134356-73-3
R-(-)-2-(4-fluorophenyl)oxirane

: 95-54-5
1,2-diamino-benzene

: 1252876-00-8
(S)-2-(4-fluorophenyl)-1,2,3,4-tetrahydroquinoxaline

Guidance literature:: With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; zinc trifluoromethanesulfonate; (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl; In toluene; at 100 ℃; for 12h; Inert atmosphere; Sealed tube;
DOI:10.1002/anie.201906199

Reference yield:

: 449-46-7
2-(4-fluorophenyl)quinoxaline

: 1287795-36-1
(R)-2-(4-fluorophenyl)-1,2,3,4-tetrahydroquinoxaline

: 1252876-00-8
(S)-2-(4-fluorophenyl)-1,2,3,4-tetrahydroquinoxaline

Guidance literature:: With {[IrH((S)-Difluorophos)]2(μ-Cl)3}+Cl-; hydrogen; In 1,4-dioxane; at 30 ℃; for 20h; under 22502.3 Torr; optical yield given as %ee; enantioselective reaction; Inert atmosphere; Autoclave;
DOI:10.1002/adsc.201000513