ethyl 2-acetamido-6-O-acetyl-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl-(1-> 6)-3,4-di O-benzoyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:ethyl 2-acetamido-6-O-acetyl-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl-(1-> 6)-3,4-di O-benzoyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside
CAS No.:1308292-84-3
Molecular Formula:C₅₄H₅₀N₂O₁₆S
Molecular Weight:1015.06
Hs Code.:

Synonyms:ethyl 2-acetamido-6-O-acetyl-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl-(1-> 6)-3,4-di O-benzoyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

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Chemical Property of ethyl 2-acetamido-6-O-acetyl-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl-(1-> 6)-3,4-di O-benzoyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

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Technology Process of ethyl 2-acetamido-6-O-acetyl-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl-(1-> 6)-3,4-di O-benzoyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

There total 5 articles about ethyl 2-acetamido-6-O-acetyl-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl-(1-> 6)-3,4-di O-benzoyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 933790-89-7
ethyl 3,4-di-O-benzoyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 1308292-81-0
2-methyl-(6-O-acetyl-3,4-di-O-benzoyl-1,2-dideoxy-α-D-glucopyrano)-[2,1-d]-2-oxazoline

: 1308292-84-3
ethyl 2-acetamido-6-O-acetyl-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl-(1-> 6)-3,4-di O-benzoyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: With trifluorormethanesulfonic acid; In dichloromethane; at 50 ℃; for 40h; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.carres.2011.02.018

Reference yield:

: C₄₈H₄₁NO₉

: 1308292-84-3
ethyl 2-acetamido-6-O-acetyl-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl-(1-> 6)-3,4-di O-benzoyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / 0.5 h / 0 - 20 °C

2: iron(III) chloride / dichloromethane / 2 h / 20 °C / Inert atmosphere

3: trifluorormethanesulfonic acid / dichloromethane / 40 h / 50 °C / Molecular sieve; Inert atmosphere

With iron(III) chloride; trifluorormethanesulfonic acid; boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1016/j.carres.2011.02.018

Reference yield:

: 1308292-83-2
C₃₁H₂₉NO₁₀

: 1308292-84-3
ethyl 2-acetamido-6-O-acetyl-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl-(1-> 6)-3,4-di O-benzoyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: iron(III) chloride / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: trifluorormethanesulfonic acid / dichloromethane / 40 h / 50 °C / Molecular sieve; Inert atmosphere

With iron(III) chloride; trifluorormethanesulfonic acid; In dichloromethane;
DOI:10.1016/j.carres.2011.02.018