pent-4-enyl 3-O-benzyl-2-deoxy-2-phthalimido-4,6-di-O-trityl-β-D-glucopyranoside

Base Information

Chemical Name:pent-4-enyl 3-O-benzyl-2-deoxy-2-phthalimido-4,6-di-O-trityl-β-D-glucopyranoside
CAS No.:188806-73-7
Molecular Formula:C₆₄H₅₇NO₇
Molecular Weight:952.159
Hs Code.:

Synonyms:pent-4-enyl 3-O-benzyl-2-deoxy-2-phthalimido-4,6-di-O-trityl-β-D-glucopyranoside

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Chemical Property of pent-4-enyl 3-O-benzyl-2-deoxy-2-phthalimido-4,6-di-O-trityl-β-D-glucopyranoside

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Technology Process of pent-4-enyl 3-O-benzyl-2-deoxy-2-phthalimido-4,6-di-O-trityl-β-D-glucopyranoside

There total 3 articles about pent-4-enyl 3-O-benzyl-2-deoxy-2-phthalimido-4,6-di-O-trityl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: triphenylmethyl perchlorate

: 338744-54-0
pent-4-enyl 3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 188806-73-7
pent-4-enyl 3-O-benzyl-2-deoxy-2-phthalimido-4,6-di-O-trityl-β-D-glucopyranoside

Guidance literature:: With 2,4,6-trimethyl-pyridine; In dichloromethane; at 20 ℃; for 20h;
DOI:10.1021/jo001477w

Reference yield: 84.0%

: 16721-97-4
trityl perchlorate

: 338744-54-0
pent-4-enyl 3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 188806-73-7
pent-4-enyl 3-O-benzyl-2-deoxy-2-phthalimido-4,6-di-O-trityl-β-D-glucopyranoside

Guidance literature:: With 2,4,6-trimethyl-pyridine; In dichloromethane;
DOI:10.1016/S0040-4039(97)00106-8

Reference yield:

: pent-4-enyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 188806-73-7
pent-4-enyl 3-O-benzyl-2-deoxy-2-phthalimido-4,6-di-O-trityl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / trifluoroacetic acid / CH₂Cl₂; H₂O / 0.17 h / 20 °C

2: 87 percent / γ-collidine / CH2Cl2 / 20 h / 20 °C

With 2,4,6-trimethyl-pyridine; trifluoroacetic acid; In dichloromethane; water;
DOI:10.1021/jo001477w