tert-butyl 2-((4-(methylsulfonamido)phenethyl)(2-(4-(methylsulfonamido)phenoxy)ethyl)amino)ethylcarbamate

Base Information

• Chemical Name: tert-butyl 2-((4-(methylsulfonamido)phenethyl)(2-(4-(methylsulfonamido)phenoxy)ethyl)amino)ethylcarbamate
• CAS No.: 944920-03-0
• Molecular Formula: C₂₅H₃₈N₄O₇S₂
• Molecular Weight: 570.731

Synonyms:tert-butyl 2-((4-(methylsulfonamido)phenethyl)(2-(4-(methylsulfonamido)phenoxy)ethyl)amino)ethylcarbamate

Chemical Property of tert-butyl 2-((4-(methylsulfonamido)phenethyl)(2-(4-(methylsulfonamido)phenoxy)ethyl)amino)ethylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of tert-butyl 2-((4-(methylsulfonamido)phenethyl)(2-(4-(methylsulfonamido)phenoxy)ethyl)amino)ethylcarbamate

There total 1 articles about tert-butyl 2-((4-(methylsulfonamido)phenethyl)(2-(4-(methylsulfonamido)phenoxy)ethyl)amino)ethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(t-butoxycarbonyl)glycinal (89711-08-0) + [Cy3B]-N-Demethyldofetilide (176447-94-2) → tert-butyl 2-((4-(methylsulfonamido)phenethyl)(2-(4-(methylsulfonamido)phenoxy)ethyl)amino)ethylcarbamate (944920-03-0)

Guidance literature:

With sodium tris(acetoxy)borohydride; In tetrahydrofuran; 1,2-dichloro-ethane; at 20 ℃;

DOI:10.1021/jm0700565

Reference yield:

tert-butyl 2-((4-(methylsulfonamido)phenethyl)(2-(4-(methylsulfonamido)phenoxy)ethyl)amino)ethylcarbamate (944920-03-0) → C51H60N6O10S3*CF3CO2H

Guidance literature:

Multi-step reaction with 2 steps

1: 0.08 h / 20 °C

2: diisopropylethylamine / dimethylformamide

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

DOI:10.1021/jm0700565

Reference yield:

tert-butyl 2-((4-(methylsulfonamido)phenethyl)(2-(4-(methylsulfonamido)phenoxy)ethyl)amino)ethylcarbamate (944920-03-0) + trifluoroacetic acid (76-05-1) → N-[4-(2-{(2-aminoethyl)[2-(4-methanesulfonylaminophenoxy)ethyl]amino}ethyl)phenyl]methanesulfonamide trifluoroacetate

Guidance literature:

at 20 ℃; for 0.0833333h;

DOI:10.1021/jm0700565

upstream raw materials:

N-(t-butoxycarbonyl)glycinal

[Cy₃B]-N-Demethyldofetilide

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