[(1S,2S,3S)-2-(3-Oxo-hexyl)-3-propyl-cyclohexyl]-carbamic acid tert-butyl ester

Base Information

Chemical Name:[(1S,2S,3S)-2-(3-Oxo-hexyl)-3-propyl-cyclohexyl]-carbamic acid tert-butyl ester
CAS No.:112680-55-4
Molecular Formula:C₂₀H₃₇NO₃
Molecular Weight:339.519
Hs Code.:

Synonyms:[(1S,2S,3S)-2-(3-Oxo-hexyl)-3-propyl-cyclohexyl]-carbamic acid tert-butyl ester

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Chemical Property of [(1S,2S,3S)-2-(3-Oxo-hexyl)-3-propyl-cyclohexyl]-carbamic acid tert-butyl ester

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Technology Process of [(1S,2S,3S)-2-(3-Oxo-hexyl)-3-propyl-cyclohexyl]-carbamic acid tert-butyl ester

There total 10 articles about [(1S,2S,3S)-2-(3-Oxo-hexyl)-3-propyl-cyclohexyl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 112680-54-3
(1S,2S,3S)-2-(3-oxo-trans-hex-1-enyl)-3-n-propyl-N-(tert-butyloxycarbonyl)cyclohexylamine

: 112680-55-4
[(1S,2S,3S)-2-(3-Oxo-hexyl)-3-propyl-cyclohexyl]-carbamic acid tert-butyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; under 760 Torr;
DOI:10.1021/jo00242a007

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 112680-55-4
[(1S,2S,3S)-2-(3-Oxo-hexyl)-3-propyl-cyclohexyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Na, 2.) 2N NaOH / 1.) NH₃

2: 87 percent / (COCl)2 / dimethylsulfoxide; CH₂Cl₂

4: 100 percent / H₂ / 5percent Pd/C / ethyl acetate / 760 Torr

With sodium hydroxide; oxalyl dichloride; hydrogen; sodium; palladium on activated charcoal; In dichloromethane; dimethyl sulfoxide; ethyl acetate;
DOI:10.1021/jo00242a007

Reference yield:

: 112680-52-1
(1S,2S,3S)-2-(hydroxymethyl)-3-n-propyl-N-(benzyloxycarbonyl)cyclohexylamine

: 112680-55-4
[(1S,2S,3S)-2-(3-Oxo-hexyl)-3-propyl-cyclohexyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / (COCl)2 / dimethylsulfoxide; CH₂Cl₂

3: 100 percent / H₂ / 5percent Pd/C / ethyl acetate / 760 Torr

With oxalyl dichloride; hydrogen; palladium on activated charcoal; In dichloromethane; dimethyl sulfoxide; ethyl acetate;
DOI:10.1021/jo00242a007