allyl (S)-4-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-3-oxopentanoate

Base Information

Chemical Name:allyl (S)-4-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-3-oxopentanoate
CAS No.:1052213-53-2
Molecular Formula:C₂₄H₂₇NO₆
Molecular Weight:425.481
Hs Code.:

Synonyms:allyl (S)-4-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-3-oxopentanoate

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Chemical Property of allyl (S)-4-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-3-oxopentanoate

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Technology Process of allyl (S)-4-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-3-oxopentanoate

There total 2 articles about allyl (S)-4-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-3-oxopentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 113240-46-3
monoallyl malonate

: 439589-23-8
(S)-2-(((benzyloxy)carbonyl)(4-methoxybenzyl)amino)propanoic acid

: 1052213-53-2
allyl (S)-4-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-3-oxopentanoate

Guidance literature:: (S)-2-(((benzyloxy)carbonyl)(4-methoxybenzyl)amino)propanoic acid; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; Inert atmosphere;

monoallyl malonate; With dibutylmagnesium; In tetrahydrofuran; n-heptane; at 0 ℃; Inert atmosphere;

In tetrahydrofuran; n-heptane; for 0.5h; Inert atmosphere;
DOI:10.1021/jo801993k

Reference yield:

: C₂₂H₂₃N₃O₄

: 113240-46-3
monoallyl malonate

: 1052213-53-2
allyl (S)-4-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-3-oxopentanoate

Guidance literature:: monoallyl malonate; With dibutylmagnesium; In tetrahydrofuran; n-heptane; at 0 ℃; Inert atmosphere;

C₂₂H₂₃N₃O₄; In tetrahydrofuran; n-heptane; for 0.5h; Inert atmosphere;
DOI:10.1021/jo801258h

Reference yield: 79.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 75-11-6
diiodomethane

: 1052213-53-2
allyl (S)-4-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-3-oxopentanoate

: 1052213-57-6
allyl (5S)-5-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-2-(hydroxymethyl)-4-oxohexanoate

Guidance literature:: diiodomethane; With diethylzinc; In hexane; dichloromethane; at 0 ℃; Inert atmosphere;

allyl (S)-4-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-3-oxopentanoate; In hexane; dichloromethane; for 0.5h; Inert atmosphere;

formaldehyd; In hexane; dichloromethane; for 0.166667h; Inert atmosphere;
DOI:10.1021/jo801993k