allyl (5S)-5-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-2-(hydroxymethyl)-4-oxohexanoate

Base Information

Chemical Name:allyl (5S)-5-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-2-(hydroxymethyl)-4-oxohexanoate
CAS No.:1052213-57-6
Molecular Formula:C₂₆H₃₁NO₇
Molecular Weight:469.535
Hs Code.:

Synonyms:allyl (5S)-5-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-2-(hydroxymethyl)-4-oxohexanoate

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Chemical Property of allyl (5S)-5-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-2-(hydroxymethyl)-4-oxohexanoate

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Technology Process of allyl (5S)-5-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-2-(hydroxymethyl)-4-oxohexanoate

There total 2 articles about allyl (5S)-5-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-2-(hydroxymethyl)-4-oxohexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 75-11-6
diiodomethane

: 1052213-53-2
allyl (S)-4-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-3-oxopentanoate

: 1052213-57-6
allyl (5S)-5-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-2-(hydroxymethyl)-4-oxohexanoate

Guidance literature:: diiodomethane; With diethylzinc; In hexane; dichloromethane; at 0 ℃; Inert atmosphere;

allyl (S)-4-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-3-oxopentanoate; In hexane; dichloromethane; for 0.5h; Inert atmosphere;

formaldehyd; In hexane; dichloromethane; for 0.166667h; Inert atmosphere;
DOI:10.1021/jo801993k

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 75-11-6
diiodomethane

: 1052213-53-2
allyl (S)-4-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-3-oxopentanoate

: 1137729-50-0
C₂₆H₃₁NO₇

: 1052213-57-6
allyl (5S)-5-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-2-(hydroxymethyl)-4-oxohexanoate

Guidance literature:: diiodomethane; allyl (S)-4-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-3-oxopentanoate; With diethylzinc; In hexane; dichloromethane; at 0 ℃; Inert atmosphere;

formaldehyd; In hexane; dichloromethane; for 0.166667h; Inert atmosphere;

With water; ammonium chloride; In hexane; dichloromethane; Inert atmosphere;
DOI:10.1021/jo801258h