5-methoxy-2-methyl-1-(phenylmethyl)-1H-indole-3-propanoic acid methyl ester

Base Information

• Chemical Name: 5-methoxy-2-methyl-1-(phenylmethyl)-1H-indole-3-propanoic acid methyl ester
• CAS No.: 163735-10-2
• Molecular Formula: C₂₁H₂₃NO₃
• Molecular Weight: 337.419

Synonyms:5-methoxy-2-methyl-1-(phenylmethyl)-1H-indole-3-propanoic acid methyl ester

Chemical Property of 5-methoxy-2-methyl-1-(phenylmethyl)-1H-indole-3-propanoic acid methyl ester

Chemical Property:

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Technology Process of 5-methoxy-2-methyl-1-(phenylmethyl)-1H-indole-3-propanoic acid methyl ester

There total 3 articles about 5-methoxy-2-methyl-1-(phenylmethyl)-1H-indole-3-propanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

5-methoxy-2-methyl-1H-indole-3-propanoic acid methyl ester (163735-09-9) + benzyl chloride (100-44-7) → 5-methoxy-2-methyl-1-(phenylmethyl)-1H-indole-3-propanoic acid methyl ester (163735-10-2)

Guidance literature:

In ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

3-(5-methoxy-2-methyl-indol-3-yl)-propionic acid (39972-31-1) → 5-methoxy-2-methyl-1-(phenylmethyl)-1H-indole-3-propanoic acid methyl ester (163735-10-2)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂SO₄ / Heating

2: NaH / dimethylformamide

With sulfuric acid; sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2007.02.038

Reference yield:

5-methoxy-2-methyl-1H-indole-3-propanoic acid methyl ester (163735-09-9) + benzyl bromide (100-39-0) → 5-methoxy-2-methyl-1-(phenylmethyl)-1H-indole-3-propanoic acid methyl ester (163735-10-2)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2007.02.038

upstream raw materials:

5-methoxy-2-methyl-1H-indole-3-propanoic acid methyl ester

benzyl bromide

3-(5-methoxy-2-methyl-indol-3-yl)-propionic acid

benzyl chloride

Downstream raw materials:

C₂₀H₂₃NO₂

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