(1-{2-oxo-2-[6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexyl]amino}ethyl)-3-{4-[tris(4-tert-butylphenyl)-methyl]phenyl}pyridinium iodide

Base Information

Chemical Name:(1-{2-oxo-2-[6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexyl]amino}ethyl)-3-{4-[tris(4-tert-butylphenyl)-methyl]phenyl}pyridinium iodide
CAS No.:1643719-06-5
Molecular Formula:C₇₃H₈₉N₂O₅*I
Molecular Weight:1201.42
Hs Code.:

(1-{2-oxo-2-[6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexyl]amino}ethyl)-3-{4-[tris(4-tert-butylphenyl)-methyl]phenyl}pyridinium iodide

Synonyms:(1-{2-oxo-2-[6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexyl]amino}ethyl)-3-{4-[tris(4-tert-butylphenyl)-methyl]phenyl}pyridinium iodide

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Chemical Property of (1-{2-oxo-2-[6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexyl]amino}ethyl)-3-{4-[tris(4-tert-butylphenyl)-methyl]phenyl}pyridinium iodide

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Technology Process of (1-{2-oxo-2-[6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexyl]amino}ethyl)-3-{4-[tris(4-tert-butylphenyl)-methyl]phenyl}pyridinium iodide

There total 14 articles about (1-{2-oxo-2-[6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexyl]amino}ethyl)-3-{4-[tris(4-tert-butylphenyl)-methyl]phenyl}pyridinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1643718-87-9
3-{4-[tris(4-tert-butylphenyl)methyl]phenyl}pyridine

: 1643719-05-4
2-chloro-N-[6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexyl]acetamide

: 1643719-06-5
(1-{2-oxo-2-[6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexyl]amino}ethyl)-3-{4-[tris(4-tert-butylphenyl)-methyl]phenyl}pyridinium iodide

Guidance literature:: With sodium iodide; In 1,4-dioxane; for 48h; Reflux;
DOI:10.1002/ejoc.201402249

Reference yield:

: 103-16-2
4-Benzyloxyphenol

: 1643719-06-5
(1-{2-oxo-2-[6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexyl]amino}ethyl)-3-{4-[tris(4-tert-butylphenyl)-methyl]phenyl}pyridinium iodide

Guidance literature:: Multi-step reaction with 11 steps

1.1: potassium carbonate / acetone / 21 h / Inert atmosphere; Reflux

2.1: N,N-dimethyl-formamide / 8 h / 70 °C / Inert atmosphere

3.1: hydrazine hydrate / dichloromethane; methanol / 17 h / 20 °C

4.1: triethylamine / dichloromethane / 19 h / 20 °C / Inert atmosphere

5.1: hydrogen; palladium 10% on activated carbon / chloroform; ethyl acetate / 23 h / 20 °C

6.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 0 °C / Inert atmosphere

6.2: 48 h / 20 °C / Inert atmosphere

7.1: hydrogen; palladium 10% on activated carbon / chloroform / 23 h / 20 °C

8.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 0 °C / Inert atmosphere

8.2: 18 h / 20 °C / Inert atmosphere

9.1: trifluoroacetic acid / dichloromethane / 19 h / 20 °C

10.1: triethylamine / dichloromethane / 4 h / -10 - 20 °C / Inert atmosphere

11.1: sodium iodide / 1,4-dioxane / 48 h / Reflux

With palladium 10% on activated carbon; hydrogen; sodium hydride; potassium carbonate; hydrazine hydrate; triethylamine; trifluoroacetic acid; sodium iodide; In 1,4-dioxane; methanol; dichloromethane; chloroform; ethyl acetate; N,N-dimethyl-formamide; acetone; 3.1: |Gabriel Amine Synthesis;
DOI:10.1002/ejoc.201402249

Reference yield:

: 56219-56-8
1-(benzyloxy)-4-(6-bromohexyloxy)benzene

: 1643719-06-5
(1-{2-oxo-2-[6-(4-{6-[4-(pent-4-ynyloxy)phenyloxy]hexyloxy}-phenyloxy)hexyl]amino}ethyl)-3-{4-[tris(4-tert-butylphenyl)-methyl]phenyl}pyridinium iodide

Guidance literature:: Multi-step reaction with 10 steps

1.1: N,N-dimethyl-formamide / 8 h / 70 °C / Inert atmosphere

2.1: hydrazine hydrate / dichloromethane; methanol / 17 h / 20 °C

3.1: triethylamine / dichloromethane / 19 h / 20 °C / Inert atmosphere

4.1: hydrogen; palladium 10% on activated carbon / chloroform; ethyl acetate / 23 h / 20 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 0 °C / Inert atmosphere

5.2: 48 h / 20 °C / Inert atmosphere

6.1: hydrogen; palladium 10% on activated carbon / chloroform / 23 h / 20 °C

7.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 0 °C / Inert atmosphere

7.2: 18 h / 20 °C / Inert atmosphere

8.1: trifluoroacetic acid / dichloromethane / 19 h / 20 °C

9.1: triethylamine / dichloromethane / 4 h / -10 - 20 °C / Inert atmosphere

10.1: sodium iodide / 1,4-dioxane / 48 h / Reflux

With palladium 10% on activated carbon; hydrogen; sodium hydride; hydrazine hydrate; triethylamine; trifluoroacetic acid; sodium iodide; In 1,4-dioxane; methanol; dichloromethane; chloroform; ethyl acetate; N,N-dimethyl-formamide; 2.1: |Gabriel Amine Synthesis;
DOI:10.1002/ejoc.201402249