benzyl 1α,3β,4β-trihydroxy-5α-<<3-(3-hydroxy-4-methoxyphenyl)propenoyl>oxy>cyclohexane-β-carboxylate

Base Information

Chemical Name:benzyl 1α,3β,4β-trihydroxy-5α-<<3-(3-hydroxy-4-methoxyphenyl)propenoyl>oxy>cyclohexane-β-carboxylate
CAS No.:76799-19-4
Molecular Formula:C₂₄H₂₆O₉
Molecular Weight:458.465
Hs Code.:

Synonyms:benzyl 1α,3β,4β-trihydroxy-5α-<<3-(3-hydroxy-4-methoxyphenyl)propenoyl>oxy>cyclohexane-β-carboxylate

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Chemical Property of benzyl 1α,3β,4β-trihydroxy-5α-<<3-(3-hydroxy-4-methoxyphenyl)propenoyl>oxy>cyclohexane-β-carboxylate

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Technology Process of benzyl 1α,3β,4β-trihydroxy-5α-<<3-(3-hydroxy-4-methoxyphenyl)propenoyl>oxy>cyclohexane-β-carboxylate

There total 3 articles about benzyl 1α,3β,4β-trihydroxy-5α-<<3-(3-hydroxy-4-methoxyphenyl)propenoyl>oxy>cyclohexane-β-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 76820-10-5
benzyl chlorogenate

: 80-48-8
methyl p-toluene sulfonate

: 76799-19-4
benzyl 1α,3β,4β-trihydroxy-5α-<<3-(3-hydroxy-4-methoxyphenyl)propenoyl>oxy>cyclohexane-β-carboxylate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 18h; Ambient temperature;
DOI:10.1021/jm00136a011

Reference yield:

: 202650-88-2
3-caffeoylquinic acid

: 76799-19-4
benzyl 1α,3β,4β-trihydroxy-5α-<<3-(3-hydroxy-4-methoxyphenyl)propenoyl>oxy>cyclohexane-β-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 38 percent / K₂CO₃ / dimethylformamide / 144 h / Ambient temperature

2: 42 percent / K₂CO₃ / dimethylformamide / 18 h / Ambient temperature

With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jm00136a011

Reference yield:

: 100-44-7
benzyl chloride

: 76799-19-4
benzyl 1α,3β,4β-trihydroxy-5α-<<3-(3-hydroxy-4-methoxyphenyl)propenoyl>oxy>cyclohexane-β-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 38 percent / K₂CO₃ / dimethylformamide / 144 h / Ambient temperature

2: 42 percent / K₂CO₃ / dimethylformamide / 18 h / Ambient temperature

With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jm00136a011