methyl 5-cyclohexa-1,3-diene-1-carboxylate

Base Information

Chemical Name:methyl 5-cyclohexa-1,3-diene-1-carboxylate
CAS No.:134039-34-2
Molecular Formula:C₁₅H₁₆N₂O₆S
Molecular Weight:352.368
Hs Code.:

methyl 5-<N-(p-nitrobenzenesulphonyl)aminomethyl>cyclohexa-1,3-diene-1-carboxylate

Synonyms:methyl 5-cyclohexa-1,3-diene-1-carboxylate

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Chemical Property of methyl 5-cyclohexa-1,3-diene-1-carboxylate

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Technology Process of methyl 5-cyclohexa-1,3-diene-1-carboxylate

There total 4 articles about methyl 5-cyclohexa-1,3-diene-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 134039-44-4
methyl 5-(aminomethyl)cyclohexa-1,3-diene-1-carboxylate

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 134039-34-2
methyl 5-cyclohexa-1,3-diene-1-carboxylate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 40h;
DOI:10.1016/S0040-4020(01)89449-7

Reference yield:

: 145264-64-8
methyl 5-cyclohexa-1,3-diene-1-carboxylate

: 134039-34-2
methyl 5-cyclohexa-1,3-diene-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / CF₃CO₂H / 0.08 h

2: 63 percent / Et₃N / tetrahydrofuran / 40 h / 20 °C

With triethylamine; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1016/S0040-4020(01)89449-7

Reference yield:

: 79356-98-2
1-tert-Butoxycarbonyl-1,2-dihydropyridine

: 134039-34-2
methyl 5-cyclohexa-1,3-diene-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

2: 90 percent / trifluoroacetic acid

3: Et₃N

With triethylamine; trifluoroacetic acid;
DOI:10.1016/S0040-4039(00)92128-2