PdC₆H₄CH₃P(C(CH₃)3)3OC(CH₃)3

Base Information

• Chemical Name: PdC₆H₄CH₃P(C(CH₃)3)3OC(CH₃)3
• CAS No.: 959930-27-9
• Molecular Formula: C₂₃H₄₃OPPd
• Molecular Weight: 472.988
• Mol file: 959930-27-9.mol

Synonyms:PdC₆H₄CH₃P(C(CH₃)3)3OC(CH₃)3

Chemical Property of PdC₆H₄CH₃P(C(CH₃)3)3OC(CH₃)3

Chemical Property:

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Technology Process of PdC₆H₄CH₃P(C(CH₃)3)3OC(CH₃)3

There total 1 articles about PdC₆H₄CH₃P(C(CH₃)3)3OC(CH₃)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[PdBr(P(tert-butyl)3)(o-tolyl)] (636583-96-5) + sodium t-butanolate (865-48-5) → PdC6H4CH3P(C(CH3)3)3OC(CH3)3 (959930-27-9)

Guidance literature:

In not given; reaction of palladium complex with alkoxide at -10°C; not isolated, detected by NMR;

DOI:10.1002/anie.200702809

Reference yield:

tri-tert-butyl phosphine (13716-12-6) + PdC6H4CH3P(C(CH3)3)3OC(CH3)3 (959930-27-9) → bis(tri-t-butylphosphine)palladium(0) (53199-31-8)

Guidance literature:

In benzene-d6; byproducts: o-C6H4CH3OC(CH3)3; warming a soln. of palladium complex with phosphine in C6D6 at 10-25°C;

DOI:10.1002/anie.200702809

upstream raw materials:

[PdBr(P(tert-butyl)3)(o-tolyl)]

sodium t-butanolate

Downstream raw materials:

bis(tri-t-butylphosphine)palladium⁽⁰⁾