4-Amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(3-methoxybut-1-yl)oxybenzamid

Base Information

Chemical Name:4-Amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(3-methoxybut-1-yl)oxybenzamid
CAS No.:114614-51-6
Molecular Formula:C₁₈H₃₀ClN₃O₃
Molecular Weight:371.907
Hs Code.:

Synonyms:4-Amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(3-methoxybut-1-yl)oxybenzamid

Suppliers and Price of 4-Amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(3-methoxybut-1-yl)oxybenzamid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(3-methoxybut-1-yl)oxybenzamid

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Technology Process of 4-Amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(3-methoxybut-1-yl)oxybenzamid

There total 3 articles about 4-Amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(3-methoxybut-1-yl)oxybenzamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 2517-43-3
3-methoxy butanol

: 38339-95-6
4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-hydroxybenzamide

: 114614-51-6
4-Amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(3-methoxybut-1-yl)oxybenzamid

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1021/jm00403a011

Reference yield:

: 2517-43-3
3-methoxy butanol

: 38339-95-6
4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-hydroxybenzamide

: 1972-28-7,218603-74-8
diethylazodicarboxylate

: 114614-51-6
4-Amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(3-methoxybut-1-yl)oxybenzamid

Guidance literature:: With ammonium hydroxide; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 364-62-5
metoclopramide

: 114614-51-6
4-Amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(3-methoxybut-1-yl)oxybenzamid

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / sodium hydride, ethanethiol / dimethylformamide / 1.5 h / 100 - 105 °C

2: 76 percent / triphenylphosphine, diethyl azodicarboxylate / tetrahydrofuran

With sodium hydride; triphenylphosphine; ethanethiol; diethylazodicarboxylate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm00403a011