succinimido 4-(2-formylphenoxy)butanoate

Base Information

• Chemical Name: succinimido 4-(2-formylphenoxy)butanoate
• CAS No.: 124856-15-1
• Molecular Formula: C₁₅H₁₅NO₆
• Molecular Weight: 305.287
• Mol file: 124856-15-1.mol

Synonyms:succinimido 4-(2-formylphenoxy)butanoate

Chemical Property of succinimido 4-(2-formylphenoxy)butanoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of succinimido 4-(2-formylphenoxy)butanoate

There total 4 articles about succinimido 4-(2-formylphenoxy)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

1-hydroxy-pyrrolidine-2,5-dione (6066-82-6) + 4-(2-formylphenoxy)butanoic acid (40359-45-3) → succinimido 4-(2-formylphenoxy)butanoate (124856-15-1)

Guidance literature:

With dicyclohexyl-carbodiimide; In 1,4-dioxane;

Reference yield:

4-(2-formylphenoxy)-butyric acid ethyl ester (40359-46-4) → succinimido 4-(2-formylphenoxy)butanoate (124856-15-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / 2.0N KOH / methanol; H₂O / 1.5 h / Heating

2: 87 percent / N,N'-dicyclohexylcarbodiimide / dioxane / 4 h

With potassium hydroxide; dicyclohexyl-carbodiimide; In 1,4-dioxane; methanol; water;

DOI:10.1002/hlca.19930760519

Reference yield:

salicylaldehyde (90-02-8) → succinimido 4-(2-formylphenoxy)butanoate (124856-15-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 93 percent / dimethylformamide / 4 h / 90 °C

2: 85 percent / 2.0N KOH / methanol; H₂O / 1.5 h / Heating

3: 87 percent / N,N'-dicyclohexylcarbodiimide / dioxane / 4 h

With potassium hydroxide; dicyclohexyl-carbodiimide; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide;

DOI:10.1002/hlca.19930760519

upstream raw materials:

1-hydroxy-pyrrolidine-2,5-dione

4-(2-formylphenoxy)butanoic acid

4-(2-formylphenoxy)-butyric acid ethyl ester

salicylaldehyde

Downstream raw materials:

1,1-diethyl-10',26'-bis<4-(2-formylphenoxy)-1-oxobutyl>-5',15',21',31',34',35',38',39'-octamethyldispirotetraoxa<10,26>diazapentacyclo<28.2.2.2^3,6.2^14,17.2^19,22>tetraconta<3,5,14,16,19,21,30,32,33,35,37,39>dodeca.>...

Refernces

• 1、 Benson, David R.,Valentekovich, Robert,Diederich, Francois. "Cyclophane als Katalysatoren: Ein Porphyrin-ueberbruecktes Cyclophan als Modell fuer Cytochrom-P-450-Enzyme". . p. 213 - 216. Retrieved 2007/10/02.