ethyl (5-allyloxy-2 tert-butyldimethylsilanyloxy-4-methoxyphenyl)-oxoacetate

Base Information

Chemical Name:ethyl (5-allyloxy-2 tert-butyldimethylsilanyloxy-4-methoxyphenyl)-oxoacetate
CAS No.:1202003-87-9
Molecular Formula:C₂₀H₃₀O₆Si
Molecular Weight:394.54
Hs Code.:

Synonyms:ethyl (5-allyloxy-2 tert-butyldimethylsilanyloxy-4-methoxyphenyl)-oxoacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (5-allyloxy-2 tert-butyldimethylsilanyloxy-4-methoxyphenyl)-oxoacetate

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Technology Process of ethyl (5-allyloxy-2 tert-butyldimethylsilanyloxy-4-methoxyphenyl)-oxoacetate

There total 1 articles about ethyl (5-allyloxy-2 tert-butyldimethylsilanyloxy-4-methoxyphenyl)-oxoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1202003-85-7
ethyl (5-allyloxy-2-hydroxy-4-methoxyphenyl)-oxoacetate

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1202003-87-9
ethyl (5-allyloxy-2 tert-butyldimethylsilanyloxy-4-methoxyphenyl)-oxoacetate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo902026s

Reference yield: 96.0%

: 1202003-87-9
ethyl (5-allyloxy-2 tert-butyldimethylsilanyloxy-4-methoxyphenyl)-oxoacetate

: 1202003-88-0
ethyl [5-allyloxy-2-(tert-butyldimethylsilanyloxy)-4-methoxyphenyl]-(hydroxyimino)acetate

Guidance literature:: With pyridine; hydroxylamine hydrochloride; In ethanol; for 1.16667h; Reflux;
DOI:10.1021/jo902026s DOI:10.1002/chem.201001036