Technology Process of C29H38N2O7
There total 7 articles about C29H38N2O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C23H27NO6; L-valine methylester hydrochloride;
With
sodium sulfate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 20 ℃;
for 0.166667h;
Inert atmosphere;
With
titanium(IV) isopropylate;
In
dichloromethane;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/jo500493c
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: (1S)-10-camphorsulfonic acid / toluene / 5 h / Reflux; Inert atmosphere
2.1: diisobutylaluminium hydride / dichloromethane / 0.25 h / -78 °C / Inert atmosphere
3.1: N-ethyl-N,N-diisopropylamine; sodium sulfate / dichloromethane / 0.17 h / 20 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
With
(1S)-10-camphorsulfonic acid; diisobutylaluminium hydride; sodium sulfate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; toluene;
DOI:10.1021/jo500493c
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: diisobutylaluminium hydride / dichloromethane / 0.25 h / -78 °C / Inert atmosphere
2.1: N-ethyl-N,N-diisopropylamine; sodium sulfate / dichloromethane / 0.17 h / 20 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere
With
diisobutylaluminium hydride; sodium sulfate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
DOI:10.1021/jo500493c