Thiophosphoric acid S-hexadecyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Base Information

Chemical Name:Thiophosphoric acid S-hexadecyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester
CAS No.:143570-25-6
Molecular Formula:C₅₇H₇₅O₈PS
Molecular Weight:951.257
Hs Code.:

Synonyms:Thiophosphoric acid S-hexadecyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Suppliers and Price of Thiophosphoric acid S-hexadecyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Thiophosphoric acid S-hexadecyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Thiophosphoric acid S-hexadecyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

There total 3 articles about Thiophosphoric acid S-hexadecyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2917-26-2
16-mercaptohexadecanoate

: 143570-25-6
Thiophosphoric acid S-hexadecyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1) n-BuLi / 1) THF, 0 deg C, 30 min, 2) room temp., 1 h

2: CH₂Cl₂ / 6 h / Ambient temperature

3: triisopropylbenzensulfonyl chloride (TPSCl), Et₃N, pyridine / 24 h / Ambient temperature

With pyridine; n-butyllithium; triisopropylbenzensulfonyl chloride; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)74812-X

Reference yield:

: 143570-23-4
Thiophosphoric acid O,O'-diethyl ester S-hexadecyl ester

: 143570-25-6
Thiophosphoric acid S-hexadecyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 6 h / Ambient temperature

2: triisopropylbenzensulfonyl chloride (TPSCl), Et₃N, pyridine / 24 h / Ambient temperature

With pyridine; triisopropylbenzensulfonyl chloride; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)74812-X

Reference yield:

: 6195-45-5,13264-84-1,22132-86-1,25018-91-1,26277-05-4,28366-79-2,30694-52-1
DL-2,3,4,5,6-penta-O-benzyl-myo-inositol

: C₂₂H₅₁O₃PSSi₂

: 143570-25-6
Thiophosphoric acid S-hexadecyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Guidance literature:: With pyridine; triisopropylbenzensulfonyl chloride; triethylamine; for 24h; Yield given; Ambient temperature;
DOI:10.1016/S0040-4039(00)74812-X