(R)-2-[1-(furan-3-yl)-1-phenylethyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:(R)-2-[1-(furan-3-yl)-1-phenylethyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1201898-95-4
Molecular Formula:C₁₈H₂₃BO₃
Molecular Weight:298.19
Hs Code.:

Synonyms:(R)-2-[1-(furan-3-yl)-1-phenylethyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of (R)-2-[1-(furan-3-yl)-1-phenylethyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of (R)-2-[1-(furan-3-yl)-1-phenylethyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 2 articles about (R)-2-[1-(furan-3-yl)-1-phenylethyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 133038-74-1
(S)-(-)-1-phenylethyl N,N-diisopropylcarbamate

: 248924-59-6
3-furylboronic acid pinacol ester

: 1201898-95-4
(R)-2-[1-(furan-3-yl)-1-phenylethyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: (S)-(-)-1-phenylethyl N,N-diisopropylcarbamate; With sec.-butyllithium; In diethyl ether; hexane; cyclohexane; at -78 - -70 ℃; for 0.25h; Inert atmosphere;

3-furylboronic acid pinacol ester; In diethyl ether; hexane; cyclohexane; at -78 ℃; for 1h; Inert atmosphere;

With magnesium bromide; In methanol; diethyl ether; hexane; cyclohexane; for 16h; Reflux; Inert atmosphere;
DOI:10.1002/anie.201402995

Reference yield: 64.0%

: 1108740-07-3
(S)-N,N-diisopropyl O-[1-(4-methoxyphenyl)]ethyl carbamate

: 248924-59-6
3-furylboronic acid pinacol ester

: 1201898-95-4
(R)-2-[1-(furan-3-yl)-1-phenylethyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: (S)-N,N-diisopropyl O-[1-(4-methoxyphenyl)]ethyl carbamate; With sec.-butyllithium; In diethyl ether; hexane; cyclohexane; at -75 - -70 ℃; for 0.416667h; Inert atmosphere;

3-furylboronic acid pinacol ester; In diethyl ether; hexane; cyclohexane; at -70 - 25 ℃; for 4.75h; Inert atmosphere;
DOI:10.1016/j.tet.2009.10.002

Reference yield: 81.0%

: 1201898-95-4
(R)-2-[1-(furan-3-yl)-1-phenylethyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 100-52-7
benzaldehyde

: 1622202-26-9
C₁₉H₁₈O₂

Guidance literature:: (R)-2-[1-(furan-3-yl)-1-phenylethyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; benzaldehyde; In tetrahydrofuran; at -78 - 20 ℃; for 16h; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 1h; enantioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201402995