(E)-3,7-dimethylocta-2,6-dien-1-yl 3-(methyl(phenyl)amino)-3-oxopropanoate

Base Information

Chemical Name:(E)-3,7-dimethylocta-2,6-dien-1-yl 3-(methyl(phenyl)amino)-3-oxopropanoate
CAS No.:1410940-60-1
Molecular Formula:C₂₀H₂₇NO₃
Molecular Weight:329.439
Hs Code.:

Synonyms:(E)-3,7-dimethylocta-2,6-dien-1-yl 3-(methyl(phenyl)amino)-3-oxopropanoate

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Chemical Property of (E)-3,7-dimethylocta-2,6-dien-1-yl 3-(methyl(phenyl)amino)-3-oxopropanoate

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Technology Process of (E)-3,7-dimethylocta-2,6-dien-1-yl 3-(methyl(phenyl)amino)-3-oxopropanoate

There total 2 articles about (E)-3,7-dimethylocta-2,6-dien-1-yl 3-(methyl(phenyl)amino)-3-oxopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-61-8
N-methylaniline

: 13947-88-1
(E)-3-(3,7-dimethyl-2,6-octadienyl-1-oxy)-3-oxopropanoic acid

: 1410940-60-1
(E)-3,7-dimethylocta-2,6-dien-1-yl 3-(methyl(phenyl)amino)-3-oxopropanoate

Guidance literature:: (E)-3-(3,7-dimethyl-2,6-octadienyl-1-oxy)-3-oxopropanoic acid; With triethylamine; In dichloromethane; at 0 ℃; for 0.0833333h; Inert atmosphere;

N-methylaniline; In tetrahydrofuran; dichloromethane; Inert atmosphere;
DOI:10.1021/ol302767w

Reference yield:

: 106-24-1
Geraniol

: 1410940-60-1
(E)-3,7-dimethylocta-2,6-dien-1-yl 3-(methyl(phenyl)amino)-3-oxopropanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene / 110 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

2.2: Inert atmosphere

With triethylamine; In dichloromethane; toluene;
DOI:10.1021/ol302767w

Reference yield: 86.0%

: 40149-83-5
2-(2-iodoethyl)isoindoline-1,3-dione

: 1410940-60-1
(E)-3,7-dimethylocta-2,6-dien-1-yl 3-(methyl(phenyl)amino)-3-oxopropanoate

: 1431884-99-9
(±)-3,7-dimethylocta-2,6-dien-1-yl 4-(1,3-dioxoisoindolin-2-yl)-(methyl(phenyl)carbamoyl)butanoate

Guidance literature:: (E)-3,7-dimethylocta-2,6-dien-1-yl 3-(methyl(phenyl)amino)-3-oxopropanoate; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h; Inert atmosphere;

2-(2-iodoethyl)isoindoline-1,3-dione; In N,N-dimethyl-formamide; at 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/ol400899e