methyl (3R,5S,8S,16E)-8-butyl-7,10-dioxo-23-phenyl-2,11-dioxa-6,9,22-triazatetracyclo[16.6.2.1-3,6-.0-21,25-]heptacosa-1⁽²⁴⁾,16,18,20,22,25-hexaene-5-carboxylate

Base Information

• Chemical Name: methyl (3R,5S,8S,16E)-8-butyl-7,10-dioxo-23-phenyl-2,11-dioxa-6,9,22-triazatetracyclo[16.6.2.1-3,6-.0-21,25-]heptacosa-1⁽²⁴⁾,16,18,20,22,25-hexaene-5-carboxylate
• CAS No.: 1020094-32-9
• Molecular Formula: C₃₄H₃₉N₃O₆
• Molecular Weight: 585.7

Synonyms:methyl (3R,5S,8S,16E)-8-butyl-7,10-dioxo-23-phenyl-2,11-dioxa-6,9,22-triazatetracyclo[16.6.2.1-3,6-.0-21,25-]heptacosa-1⁽²⁴⁾,16,18,20,22,25-hexaene-5-carboxylate

Chemical Property of methyl (3R,5S,8S,16E)-8-butyl-7,10-dioxo-23-phenyl-2,11-dioxa-6,9,22-triazatetracyclo[16.6.2.1-3,6-.0-21,25-]heptacosa-1⁽²⁴⁾,16,18,20,22,25-hexaene-5-carboxylate

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Technology Process of methyl (3R,5S,8S,16E)-8-butyl-7,10-dioxo-23-phenyl-2,11-dioxa-6,9,22-triazatetracyclo[16.6.2.1-3,6-.0-21,25-]heptacosa-1⁽²⁴⁾,16,18,20,22,25-hexaene-5-carboxylate

There total 1 articles about methyl (3R,5S,8S,16E)-8-butyl-7,10-dioxo-23-phenyl-2,11-dioxa-6,9,22-triazatetracyclo[16.6.2.1-3,6-.0-21,25-]heptacosa-1⁽²⁴⁾,16,18,20,22,25-hexaene-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

methyl N-[(hex-5-en-1-yloxy)carbonyl]-L-norleucyl-(4R)-4-[(2-phenyl-6-vinylquinolin-4-yl)oxy]-L-prolinate (1020094-24-9) → methyl (3R,5S,8S,16E)-8-butyl-7,10-dioxo-23-phenyl-2,11-dioxa-6,9,22-triazatetracyclo[16.6.2.1-3,6-.0-21,25-]heptacosa-1(24),16,18,20,22,25-hexaene-5-carboxylate (1020094-32-9)

Guidance literature:

bis(Me₃Ph)imidazole[(iPrO)(Me₂NSO₂)Ph]methyleneRu(II)Cl₂; In 1,2-dichloro-ethane; at 20 ℃; for 24h;

DOI:10.1021/ja711120r

Reference yield:

methyl (3R,5S,8S,16E)-8-butyl-7,10-dioxo-23-phenyl-2,11-dioxa-6,9,22-triazatetracyclo[16.6.2.1-3,6-.0-21,25-]heptacosa-1(24),16,18,20,22,25-hexaene-5-carboxylate (1020094-32-9) → C34H41N3O6

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; at 20 ℃; for 1h; under 760.051 Torr;

DOI:10.1021/ja711120r

upstream raw materials:

methyl N-[(hex-5-en-1-yloxy)carbonyl]-L-norleucyl-(4R)-4-[(2-phenyl-6-vinylquinolin-4-yl)oxy]-L-prolinate

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