2-(3-Hydroxy-3-methyl-but-1-ynyl)-benzoic acid

Base Information

Chemical Name:2-(3-Hydroxy-3-methyl-but-1-ynyl)-benzoic acid
CAS No.:147454-79-3
Molecular Formula:C₁₂H₁₂O₃
Molecular Weight:204.225
Hs Code.:

Synonyms:2-(3-Hydroxy-3-methyl-but-1-ynyl)-benzoic acid

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Chemical Property of 2-(3-Hydroxy-3-methyl-but-1-ynyl)-benzoic acid

Chemical Property:

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Technology Process of 2-(3-Hydroxy-3-methyl-but-1-ynyl)-benzoic acid

There total 3 articles about 2-(3-Hydroxy-3-methyl-but-1-ynyl)-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88-67-5
2-Iodobenzoic acid

: 147454-79-3
2-(3-Hydroxy-3-methyl-but-1-ynyl)-benzoic acid

: 147454-71-5
(Z)-3-(2-hydroxy-2-methylpropylidene)-3H-isobenzofuran-1-one

: 115-19-5
2-methyl-but-3-yn-2-ol

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) DMF, 1 h, 2.) DMF, a) RT, 1 h, b) 30 deg C, 6 h;
DOI:10.1039/c39930000086

Reference yield:

: 88-67-5
2-Iodobenzoic acid

: 115-19-5
2-methyl-but-3-yn-2-ol

: 147454-79-3
2-(3-Hydroxy-3-methyl-but-1-ynyl)-benzoic acid

Guidance literature:: With triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In N,N-dimethyl-formamide; for 6h; Ambient temperature;
DOI:10.1039/a705450e

Reference yield:

: 88-67-5
2-Iodobenzoic acid

: 115-19-5
2-methyl-but-3-yn-2-ol

: 147454-79-3
2-(3-Hydroxy-3-methyl-but-1-ynyl)-benzoic acid

: 3-(1-hydroxy-1-methylethyl)-isochromen-1-one

: 147454-71-5
(Z)-3-(2-hydroxy-2-methylpropylidene)-3H-isobenzofuran-1-one

Guidance literature:: With tetrabutyl-ammonium chloride; potassium acetate; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In N,N-dimethyl-formamide; at 30 ℃; for 6h; other catalyst, base, solvents, temperature and time;
DOI:10.1039/a705450e