Trimethyl-stibin-sulfid

Base Information

• Chemical Name: Trimethyl-stibin-sulfid
• CAS No.: 15082-93-6
• Molecular Formula: C₃H₉SSb
• Molecular Weight: 198.92
• Mol file: 15082-93-6.mol

Synonyms:Trimethyl-stibin-sulfid

Chemical Property of Trimethyl-stibin-sulfid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of Trimethyl-stibin-sulfid

There total 1 articles about Trimethyl-stibin-sulfid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

((CH3)3SbS)2(CH3)2SnCl2 → 2,2,4,4,6,6-hexamethyl-1,3,5,2,4,6-trithiatristanninane (16892-64-1) + trimethylantimony dichloride (13059-67-1,22810-79-3,91108-42-8) + Trimethyl-stibin-sulfid (15082-93-6)

Guidance literature:

In chloroform-d1; reversible dissociation in soln.; monitored by (119)Sn, (13)C NMR spectroscopy;

DOI:10.1002/zaac.200300102

Reference yield: 90.0%

Trimethyl-stibin-sulfid (15082-93-6) → trimethylantimony (594-10-5)

Guidance literature:

With (C₆H₅CH₂)6Sn₂; In chloroform; byproducts: hexaorganodistannathian; refluxing for 1 h;

DOI:10.1016/S0022-328X(00)87774-8

Reference yield:

antimony(V) chloride (7647-18-9) + Trimethyl-stibin-sulfid (15082-93-6) → trimethylantimony dichloride (13059-67-1,22810-79-3,91108-42-8)

Guidance literature:

In tetrachloromethane; under N2; SbCl5 reacted with Me3SbS (molar ratio 1:1) in CCl4 at -20°C; detd. by IR and (1)H NMR spectra; mixt. of Me3SbS, Me3SbCl2 and minor unidentified compd. obtained;

DOI:10.1016/j.ica.2004.10.039

Downstream raw materials:

trimethylantimony dichloride

trimethylantimony