4,6-Di-O-acetyl-2,3-dideoxy-5-O-(p-nitrobenzoyl)-aldehydo-D-erythro-trans-hex-2-enose

Base Information

Chemical Name:4,6-Di-O-acetyl-2,3-dideoxy-5-O-(p-nitrobenzoyl)-aldehydo-D-erythro-trans-hex-2-enose
CAS No.:128599-92-8
Molecular Formula:C₁₇H₁₇NO₉
Molecular Weight:379.323
Hs Code.:

Synonyms:4,6-Di-O-acetyl-2,3-dideoxy-5-O-(p-nitrobenzoyl)-aldehydo-D-erythro-trans-hex-2-enose

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Chemical Property of 4,6-Di-O-acetyl-2,3-dideoxy-5-O-(p-nitrobenzoyl)-aldehydo-D-erythro-trans-hex-2-enose

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Technology Process of 4,6-Di-O-acetyl-2,3-dideoxy-5-O-(p-nitrobenzoyl)-aldehydo-D-erythro-trans-hex-2-enose

There total 1 articles about 4,6-Di-O-acetyl-2,3-dideoxy-5-O-(p-nitrobenzoyl)-aldehydo-D-erythro-trans-hex-2-enose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 29581-05-3
(2E,4S,5R)-4,6-diacetoxy-5-hydroxy-2(E)-hexenal

: 122-04-3
4-nitro-benzoyl chloride

: 128599-92-8
4,6-Di-O-acetyl-2,3-dideoxy-5-O-(p-nitrobenzoyl)-aldehydo-D-erythro-trans-hex-2-enose

Guidance literature:: With pyridine; In 1,4-dioxane; at 25 ℃; for 24h;

Reference yield: 75.0%

: 128599-92-8
4,6-Di-O-acetyl-2,3-dideoxy-5-O-(p-nitrobenzoyl)-aldehydo-D-erythro-trans-hex-2-enose

: 128599-93-9
(4S,5R)-4,6-Diacetoxy-3-azido-5-(p-nitrobenzoyloxy)hexanal

Guidance literature:: With sodium azide; acetic acid; 1) 0.5 h, 0 deg C 2) 18 h, r.t.;

Reference yield:

: 128599-92-8
4,6-Di-O-acetyl-2,3-dideoxy-5-O-(p-nitrobenzoyl)-aldehydo-D-erythro-trans-hex-2-enose

: 128599-94-0
Methyl 4-O-acetyl-3-azido-2,3-dideoxy-6-O-(p-nitrobenzoyl)-β-D-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / NaN₃, glacial AcOH / 1) 0.5 h, 0 deg C 2) 18 h, r.t.

2: 4 percent / HCl / methanol / 20 h / Ambient temperature

With hydrogenchloride; sodium azide; acetic acid; In methanol;