Technology Process of C26H35N5O4
There total 5 articles about C26H35N5O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(ll) sulfate pentahydrate; copper;
In
tetrahydrofuran; water;
at 25 ℃;
for 12h;
Inert atmosphere;
DOI:10.1021/ja1071916
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 4-toluenesulfonyl azide; potassium carbonate / acetonitrile / 2 h / 25 °C / Inert atmosphere
1.2: 12 h / 25 °C / Inert atmosphere
2.1: copper(ll) sulfate pentahydrate; copper / tetrahydrofuran; water / 12 h / 25 °C / Inert atmosphere
With
4-toluenesulfonyl azide; copper(ll) sulfate pentahydrate; copper; potassium carbonate;
In
tetrahydrofuran; water; acetonitrile;
1.1: Ohira-Bestmann reaction / 1.2: Ohira-Bestmann reaction;
DOI:10.1021/ja1071916
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: copper(ll) sulfate pentahydrate; triflic azide; potassium carbonate / methanol; dichloromethane / 12 h / 25 °C / Inert atmosphere
2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.33 h / 0 °C / Inert atmosphere
2.2: 12 h / 0 - 25 °C / Inert atmosphere
3.1: copper(ll) sulfate pentahydrate; copper / tetrahydrofuran; water / 12 h / 25 °C / Inert atmosphere
With
copper(ll) sulfate pentahydrate; triflic azide; copper; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/ja1071916
