C₂₃H₂₅FN₂O₄

Base Information

Chemical Name:C₂₃H₂₅FN₂O₄
CAS No.:1338350-74-5
Molecular Formula:C₂₃H₂₅FN₂O₄
Molecular Weight:412.461
Hs Code.:

C<sub>23</sub>H<sub>25</sub>FN<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₃H₂₅FN₂O₄

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Chemical Property of C₂₃H₂₅FN₂O₄

Chemical Property:

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Technology Process of C₂₃H₂₅FN₂O₄

There total 9 articles about C₂₃H₂₅FN₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 55601-20-2
β-fluoro-β-phenylamine

: 1338350-70-1
C₁₅H₁₆ClNO₄

: 1338350-74-5
C₂₃H₂₅FN₂O₄

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 0.5h;
DOI:10.1016/j.bmc.2011.07.062

Reference yield:

: 621-59-0
isovanillin

: 1338350-74-5
C₂₃H₂₅FN₂O₄

Guidance literature:: Multi-step reaction with 7 steps

1: nitronium tetrafluoborate / dichloromethane / 24 h / -20 °C / Inert atmosphere

2: caesium carbonate; sodium iodide / N,N-dimethyl-formamide / 25 h / 20 - 80 °C / Inert atmosphere

3: hydrogenchloride; iron; acetic acid / water; ethyl acetate / 0.25 h / Reflux

4: piperidine; acetic acid / ethanol / 16 h / Reflux; Inert atmosphere

5: hydrogenchloride; water / ethanol / 60 °C

6: thionyl chloride / toluene / 3 h / Reflux; Inert atmosphere

7: triethylamine / dichloromethane / 0.5 h / 0 - 20 °C

With piperidine; hydrogenchloride; thionyl chloride; nitronium tetrafluoborate; water; iron; caesium carbonate; acetic acid; triethylamine; sodium iodide; In ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmc.2011.07.062

Reference yield:

: 282089-63-8
8-butoxy-7-methoxy-2-oxo-1,2-dihydroquinoline-3-carboxylic acid

: 1338350-74-5
C₂₃H₂₅FN₂O₄

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / toluene / 3 h / Reflux; Inert atmosphere

2: triethylamine / dichloromethane / 0.5 h / 0 - 20 °C

With thionyl chloride; triethylamine; In dichloromethane; toluene;
DOI:10.1016/j.bmc.2011.07.062