2,4-diallyl-4-methylcyclohexa-2,5-dien-1-one

Base Information

Chemical Name:2,4-diallyl-4-methylcyclohexa-2,5-dien-1-one
CAS No.:2059-44-1
Molecular Formula:C₁₃H₁₆O
Molecular Weight:188.269
Hs Code.:

Synonyms:2,4-diallyl-4-methylcyclohexa-2,5-dien-1-one

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Chemical Property of 2,4-diallyl-4-methylcyclohexa-2,5-dien-1-one

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Technology Process of 2,4-diallyl-4-methylcyclohexa-2,5-dien-1-one

There total 4 articles about 2,4-diallyl-4-methylcyclohexa-2,5-dien-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₁₈

: 2059-44-1
2,4-diallyl-4-methylcyclohexa-2,5-dien-1-one

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; at 0 - 20 ℃; Inert atmosphere; Saturated solution;
DOI:10.1246/cl.200216

Reference yield:

: 1-(2-bromo-4-methylphenyl)-N,N,N-trimethylmethanaminium iodide

: 2059-44-1
2,4-diallyl-4-methylcyclohexa-2,5-dien-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; cesium fluoride / acetone / 12 h / 60 °C / Inert atmosphere; Sealed tube

2: 3-chloro-benzenecarboperoxoic acid; sodium hydrogencarbonate / dichloromethane; water / 0 - 20 °C / Inert atmosphere; Saturated solution

With palladium diacetate; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; cesium fluoride; bis[2-(diphenylphosphino)phenyl] ether; In dichloromethane; water; acetone;
DOI:10.1246/cl.200216

Reference yield:

: 4052-88-4
4-methyl-N,N-dimethylbenzylamine

: 2059-44-1
2,4-diallyl-4-methylcyclohexa-2,5-dien-1-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / diethyl ether; hexane / 18 h / -78 - 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: acetonitrile / 20 °C / Inert atmosphere

3.1: palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; cesium fluoride / acetone / 12 h / 60 °C / Inert atmosphere; Sealed tube

4.1: 3-chloro-benzenecarboperoxoic acid; sodium hydrogencarbonate / dichloromethane; water / 0 - 20 °C / Inert atmosphere; Saturated solution

With n-butyllithium; palladium diacetate; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; cesium fluoride; bis[2-(diphenylphosphino)phenyl] ether; In diethyl ether; hexane; dichloromethane; water; acetone; acetonitrile;
DOI:10.1246/cl.200216