(-)-[(1-cyclohexylallyloxy)methyl]benzene

Base Information

Chemical Name:(-)-[(1-cyclohexylallyloxy)methyl]benzene
CAS No.:1021903-12-7
Molecular Formula:C₁₆H₂₂O
Molecular Weight:230.35
Hs Code.:

Synonyms:(-)-[(1-cyclohexylallyloxy)methyl]benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-[(1-cyclohexylallyloxy)methyl]benzene

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Technology Process of (-)-[(1-cyclohexylallyloxy)methyl]benzene

There total 2 articles about (-)-[(1-cyclohexylallyloxy)methyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 172990-75-9
1-acetoxy-3-cyclohexyl-trans-2-propene

: 100-51-6,185532-71-2
benzyl alcohol

: 1021903-12-7
(-)-[(1-cyclohexylallyloxy)methyl]benzene

: 144222-05-9
(+)-[(1-cyclohexylallyloxy)methyl]benzene

: 146330-83-8
trans-1-(benzyloxy)-3-cyclohexyl-2-propene

Guidance literature:: With 1-Phenylprop-1-yne; potassium phosphate; chiral binaphthyl-derived phosphoramidite iridium complex; In toluene; at 23 ℃; Title compound not separated from byproducts.;
DOI:10.1002/anie.200705267

Reference yield:

: 4352-44-7
1-cyclohexylprop-2-en-1-ol

: 100-51-6,185532-71-2
benzyl alcohol

: 1021903-12-7
(-)-[(1-cyclohexylallyloxy)methyl]benzene

: 144222-05-9
(+)-[(1-cyclohexylallyloxy)methyl]benzene

Guidance literature:: With bis(1,5-cyclooctadiene)diiridium(I) dichloride; 5-(dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-yl)-5H-dibenzo[b,f]azepine; 3-chlorobenzoate; In 1,2-dichloro-ethane; at 50 ℃; for 168h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201007716

Reference yield:

: 1021903-12-7
(-)-[(1-cyclohexylallyloxy)methyl]benzene

: 1021903-20-7
(+)-3-benzyloxy-3-cyclohexylpropan-1-ol

Guidance literature:: (-)-[(1-cyclohexylallyloxy)methyl]benzene; With borane; In tetrahydrofuran; at 0 ℃; for 1h;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; at 20 ℃; for 1h; Further stages.;
DOI:10.1002/anie.200705267