1-(furan-2-yl)vinyl cyclohexa-1,3-dienecarboxylate

Base Information

Chemical Name:1-(furan-2-yl)vinyl cyclohexa-1,3-dienecarboxylate
CAS No.:1627214-63-4
Molecular Formula:C₁₃H₁₂O₃
Molecular Weight:216.236
Hs Code.:

Synonyms:1-(furan-2-yl)vinyl cyclohexa-1,3-dienecarboxylate

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Chemical Property of 1-(furan-2-yl)vinyl cyclohexa-1,3-dienecarboxylate

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Technology Process of 1-(furan-2-yl)vinyl cyclohexa-1,3-dienecarboxylate

There total 2 articles about 1-(furan-2-yl)vinyl cyclohexa-1,3-dienecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 62889-08-1
1-(2-furyl)-1-(trimethylsilyloxy)ethylene

: C₇H₇FO

: 1627214-63-4
1-(furan-2-yl)vinyl cyclohexa-1,3-dienecarboxylate

Guidance literature:: With dmap; In acetonitrile; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201402067

Reference yield:

: 2206-65-7
cyclohexa-1,3-diene-1-carboxylic acid

: 1627214-63-4
1-(furan-2-yl)vinyl cyclohexa-1,3-dienecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: diethylamino-sulfur trifluoride / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

2: dmap / acetonitrile / 1 h / 20 °C / Inert atmosphere

With dmap; diethylamino-sulfur trifluoride; In dichloromethane; acetonitrile;
DOI:10.1002/anie.201402067