1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-1,3,2',2',6'-pentadeaminoparomomycin

Base Information

• Chemical Name: 1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-1,3,2',2',6'-pentadeaminoparomomycin
• CAS No.: 1073243-62-5
• Molecular Formula: C₆₅H₇₁N₁₅O₁₄
• Molecular Weight: 1286.37

Synonyms:1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-1,3,2',2',6'-pentadeaminoparomomycin

Chemical Property of 1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-1,3,2',2',6'-pentadeaminoparomomycin

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Technology Process of 1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-1,3,2',2',6'-pentadeaminoparomomycin

There total 1 articles about 1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-1,3,2',2',6'-pentadeaminoparomomycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-4',6'-O-benzylidene-1,3,2',2',6'-pentadeaminoparomomycin (1073243-50-1) → 1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-1,3,2',2',6'-pentadeaminoparomomycin (1073243-62-5)

Guidance literature:

With p-toluenesulfonic acid monohydrate; In methanol;

DOI:10.1021/acs.joc.0c00743

Reference yield: 99.0%

1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-1,3,2',2',6'-pentadeaminoparomomycin (1073243-62-5) → 1,3,2’,2’‘‘,6’‘‘-pentaazido-6,3’,2’‘,5’‘,3’‘‘,4’‘‘-hexa-O-benzyl-1,3,2’,2’‘‘,6’‘‘-pentadeaminoparomomycin-6’-carboxylic acid

Guidance literature:

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; In water; acetonitrile; for 3.5h;

DOI:10.1021/acs.joc.0c01836

Reference yield: 83.0%

1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-1,3,2',2',6'-pentadeaminoparomomycin (1073243-62-5) + triisopropylsilyl trifluoromethanesulfonate (80522-42-5) → 1,3,2’,2’‘‘,6’‘‘-pentaazido-6,3’,2’‘,5’‘,3’‘‘,4’‘‘-hexa-O-benzyl-6’-O-triisopropylsilyl-1,3,2’,2’‘‘,6’‘‘-pentadeaminoparomomycin

Guidance literature:

With 2,6-dimethylpyridine; In dichloromethane;

upstream raw materials:

1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-4',6'-O-benzylidene-1,3,2',2',6'-pentadeaminoparomomycin

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