1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-4',6'-O-benzylidene-1,3,2',2',6'-pentadeaminoparomomycin

Base Information

Chemical Name:1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-4',6'-O-benzylidene-1,3,2',2',6'-pentadeaminoparomomycin
CAS No.:1073243-50-1
Molecular Formula:C₇₂H₇₅N₁₅O₁₄
Molecular Weight:1374.48
Hs Code.:

Synonyms:1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-4',6'-O-benzylidene-1,3,2',2',6'-pentadeaminoparomomycin

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Chemical Property of 1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-4',6'-O-benzylidene-1,3,2',2',6'-pentadeaminoparomomycin

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Technology Process of 1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-4',6'-O-benzylidene-1,3,2',2',6'-pentadeaminoparomomycin

There total 1 articles about 1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-4',6'-O-benzylidene-1,3,2',2',6'-pentadeaminoparomomycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 875125-34-1
4',6‘-O-benzylidene-1,2',2''',3,6'''-pentaazidoparomomycin

: 100-39-0
benzyl bromide

: 1073243-50-1
1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-4',6'-O-benzylidene-1,3,2',2',6'-pentadeaminoparomomycin

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 26 ℃; for 28h; Inert atmosphere;
DOI:10.1002/hlca.200890167

Reference yield: 87.0%

: 1073243-50-1
1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-4',6'-O-benzylidene-1,3,2',2',6'-pentadeaminoparomomycin

: 927812-19-9
6,3',4',2'',5'',3''',4'''-hepta-O-benzyl-1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazidoparomomycin

Guidance literature:: With dimethylsulfide borane complex; di-n-butylboryl trifluoromethanesulfonate; In dichloromethane; at 0 - 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jacs.7b07754