α-<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>-3-methyl-5-isoxazoleethanol

Base Information

Chemical Name:α-<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>-3-methyl-5-isoxazoleethanol
CAS No.:113465-77-3
Molecular Formula:C₂₀H₂₉NO₃
Molecular Weight:331.455
Hs Code.:

Synonyms:α-<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>-3-methyl-5-isoxazoleethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>-3-methyl-5-isoxazoleethanol

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Technology Process of α-<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>-3-methyl-5-isoxazoleethanol

There total 3 articles about α-<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>-3-methyl-5-isoxazoleethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 5-isoxazoleethanol

: 113465-77-3
α-<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>-3-methyl-5-isoxazoleethanol

Guidance literature:

Reference yield:

: 1620-98-0
3,5-di-t-butyl-4-hydroxybenzaldehyde

: 113465-77-3
α-<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>-3-methyl-5-isoxazoleethanol

Guidance literature:: 3,5-dimethyl-1,2-oxazole; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1.75h;

3,5-di-t-butyl-4-hydroxybenzaldehyde; In tetrahydrofuran; at -78 ℃; for 5.5h;

Reference yield:

: 300-87-8
3,5-dimethyl-1,2-oxazole

: 1620-98-0
3,5-di-t-butyl-4-hydroxybenzaldehyde

: 113465-77-3
α-<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>-3-methyl-5-isoxazoleethanol

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) THF, hexane, -78 deg C, 2 h, 2.) RT, 8 h;
DOI:10.1021/jm00106a006