Si,Si'-dichloro-Si,Si'-dimethyl-Si,Si'-diphenyl-Si,Si'-propane-1,3-diyl-bis-silane

Base Information

• Chemical Name: Si,Si'-dichloro-Si,Si'-dimethyl-Si,Si'-diphenyl-Si,Si'-propane-1,3-diyl-bis-silane
• CAS No.: 53722-12-6
• Molecular Formula: C₁₇H₂₂Cl₂Si₂
• Molecular Weight: 353.439
• Mol file: 53722-12-6.mol

Synonyms:Si,Si'-dichloro-Si,Si'-dimethyl-Si,Si'-diphenyl-Si,Si'-propane-1,3-diyl-bis-silane

Chemical Property of Si,Si'-dichloro-Si,Si'-dimethyl-Si,Si'-diphenyl-Si,Si'-propane-1,3-diyl-bis-silane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Si,Si'-dichloro-Si,Si'-dimethyl-Si,Si'-diphenyl-Si,Si'-propane-1,3-diyl-bis-silane

There total 1 articles about Si,Si'-dichloro-Si,Si'-dimethyl-Si,Si'-diphenyl-Si,Si'-propane-1,3-diyl-bis-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

chloro(methyl)phenylsilane (1631-82-9) + allylchloro(methyl)phenylsilane (112945-35-4) → Si,Si'-dichloro-Si,Si'-dimethyl-Si,Si'-diphenyl-Si,Si'-propane-1,3-diyl-bis-silane (53722-12-6)

Guidance literature:

With dihydrogen hexachloroplatinate; In isopropyl alcohol; at 80 ℃;

DOI:10.1007/bf01169967

Reference yield:

Si,Si'-dichloro-Si,Si'-dimethyl-Si,Si'-diphenyl-Si,Si'-propane-1,3-diyl-bis-silane (53722-12-6) → (2R,6S)-2,6-Dimethyl-2,6-diphenyl-[1,2,6]oxadisilinane + (2S,6S)-2,6-Dimethyl-2,6-diphenyl-[1,2,6]oxadisilinane

Guidance literature:

With pyridine; water; In 1,4-dioxane; diethyl ether; for 2h; Title compound not separated from byproducts;

DOI:10.1007/bf01169967

upstream raw materials:

chloro(methyl)phenylsilane

allylchloro(methyl)phenylsilane