allylchloro(methyl)phenylsilane

Base Information

Chemical Name:allylchloro(methyl)phenylsilane
CAS No.:112945-35-4
Molecular Formula:C₁₀H₁₃ClSi
Molecular Weight:196.752
Hs Code.:

Synonyms:allylchloro(methyl)phenylsilane

Suppliers and Price of allylchloro(methyl)phenylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allylchloro(methyl)phenylsilane

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of allylchloro(methyl)phenylsilane

There total 3 articles about allylchloro(methyl)phenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 346713-20-0
allylsamarium bromide

: 149-74-6
dichloromethylphenylsilane

: 112945-35-4
allylchloro(methyl)phenylsilane

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1016/j.jorganchem.2006.07.023

Reference yield: 42.0%

: 7072-26-6,111949-34-9
allyl(methyl)(phenyl)silane

: 112945-35-4
allylchloro(methyl)phenylsilane

Guidance literature:: With copper(l) iodide; copper dichloride; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1021/acs.organomet.9b00498

Reference yield:

: 1631-82-9
chloro(methyl)phenylsilane

: 112945-35-4
allylchloro(methyl)phenylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium / diethyl ether / 1 h / 45 °C / Inert atmosphere; Glovebox

1.2: 20 °C / Inert atmosphere; Glovebox

2.1: copper dichloride; copper(l) iodide / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere; Schlenk technique; Sealed tube

With copper(l) iodide; magnesium; copper dichloride; In tetrahydrofuran; diethyl ether;
DOI:10.1021/acs.organomet.9b00498